2-chloro-4-[(4-methylphenyl)sulfonyl]phenanthridine

Base Information

Chemical Name:2-chloro-4-[(4-methylphenyl)sulfonyl]phenanthridine
CAS No.:1322074-88-3
Molecular Formula:C₂₀H₁₄ClNO₂S
Molecular Weight:367.856
Hs Code.:

Synonyms:

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Chemical Property of 2-chloro-4-[(4-methylphenyl)sulfonyl]phenanthridine

Chemical Property:

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Technology Process of 2-chloro-4-[(4-methylphenyl)sulfonyl]phenanthridine

There total 5 articles about 2-chloro-4-[(4-methylphenyl)sulfonyl]phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27353-44-2
2-chlorophenanthridin-6(5H)-one

: 1322074-88-3
2-chloro-4-[(4-methylphenyl)sulfonyl]phenanthridine

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / Reflux

2: pyridine / 0 °C

3: sulfuric acid / 0.05 h / 105 °C

With pyridine; lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran;
DOI:10.1080/00397911.2010.515329

Reference yield:

: 486-25-9,952573-42-1
9-fluorenone

: 1322074-88-3
2-chloro-4-[(4-methylphenyl)sulfonyl]phenanthridine

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine; hydroxylamine hydrochloride / methanol / 1.5 h / Reflux

2: polyphosphoric acid / 20 - 180 °C

3: sulfuryl dichloride / benzene / 3 h / Reflux

4: lithium aluminium tetrahydride / tetrahydrofuran / Reflux

5: pyridine / 0 °C

6: sulfuric acid / 0.05 h / 105 °C

With pyridine; lithium aluminium tetrahydride; sulfuryl dichloride; sulfuric acid; hydroxylamine hydrochloride; In tetrahydrofuran; methanol; benzene; 2: Beckmann rearrangement;
DOI:10.1080/00397911.2010.515329

Reference yield:

: 1015-89-0
6(5H)-phenanthridinone

: 1322074-88-3
2-chloro-4-[(4-methylphenyl)sulfonyl]phenanthridine

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuryl dichloride / benzene / 3 h / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / Reflux

3: pyridine / 0 °C

4: sulfuric acid / 0.05 h / 105 °C

With pyridine; lithium aluminium tetrahydride; sulfuryl dichloride; sulfuric acid; In tetrahydrofuran; benzene;
DOI:10.1080/00397911.2010.515329