C₂₇H₂₅FN₅O₇P

Base Information

Chemical Name:C₂₇H₂₅FN₅O₇P
CAS No.:1048373-89-2
Molecular Formula:C₂₇H₂₅FN₅O₇P
Molecular Weight:581.497
Hs Code.:

C<sub>27</sub>H<sub>25</sub>FN<sub>5</sub>O<sub>7</sub>P

Synonyms:

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Chemical Property of C₂₇H₂₅FN₅O₇P

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Technology Process of C₂₇H₂₅FN₅O₇P

There total 5 articles about C₂₇H₂₅FN₅O₇P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 16001-93-7
tetramethyl methylenediphosphonate

: 1048373-86-9
C₂₄H₂₀FN₅O₅

: 1048373-89-2
C₂₇H₂₅FN₅O₇P

Guidance literature:: C₂₄H₂₀FN₅O₅; With pyridinium trifluroacetate; dicyclohexyl-carbodiimide; In dimethyl sulfoxide; at 20 ℃; for 18h;

tetramethyl methylenediphosphonate; With potassium tert-butylate; In dimethyl sulfoxide; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2013.03.095

Reference yield:

: C₃₀H₂₈FN₅O₃

: 1048373-89-2
C₂₇H₂₅FN₅O₇P

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 18 h / 20 °C

2.1: acetic acid / 48 h / 50 °C

3.1: pyridinium trifluroacetate; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 18 h / 20 °C

3.2: 1 h / 0 - 20 °C

With pyridine; pyridinium trifluroacetate; acetic acid; dicyclohexyl-carbodiimide; In dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2013.03.095

Reference yield:

: C₄₄H₃₆FN₅O₅

: 1048373-89-2
C₂₇H₂₅FN₅O₇P

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / 48 h / 50 °C

2.1: pyridinium trifluroacetate; dicyclohexyl-carbodiimide / dimethyl sulfoxide / 18 h / 20 °C

2.2: 1 h / 0 - 20 °C

With pyridinium trifluroacetate; acetic acid; dicyclohexyl-carbodiimide; In dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2013.03.095