C₁₄H₁₈O₃

Base Information

Chemical Name:C₁₄H₁₈O₃
CAS No.:1449770-01-7
Molecular Formula:C₁₄H₁₈O₃
Molecular Weight:234.295
Hs Code.:

C<sub>14</sub>H<sub>18</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₁₄H₁₈O₃

Chemical Property:

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Technology Process of C₁₄H₁₈O₃

There total 5 articles about C₁₄H₁₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1423043-19-9
1-(4-((tert-butyldimethylsilyl)oxy)phenyl)but-3-yn-1-ol

: 1449770-01-7
C₁₄H₁₈O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 0 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / Inert atmosphere

4.1: bis-[(trifluoroacetoxy)iodo]benzene; sodium hydrogencarbonate / 0.5 h / 0 °C / Inert atmosphere

With triethylsilane; n-butyllithium; lithium hydroxide monohydrate; boron trifluoride diethyl etherate; sodium hydrogencarbonate; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob27491h

Reference yield:

: 1449770-11-9
C₁₉H₃₀O₂Si

: 1449770-01-7
C₁₄H₁₈O₃

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / Inert atmosphere

2: bis-[(trifluoroacetoxy)iodo]benzene; sodium hydrogencarbonate / 0.5 h / 0 °C / Inert atmosphere

With lithium hydroxide monohydrate; sodium hydrogencarbonate; bis-[(trifluoroacetoxy)iodo]benzene; In N,N-dimethyl-formamide;
DOI:10.1039/c3ob27491h

Reference yield:

: 120743-99-9
p-[(tert-butyldimethylsilyl)oxy]benzaldehyde

: 1449770-01-7
C₁₄H₁₈O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: titanium tetrachloride; zinc / tetrahydrofuran; dichloromethane; toluene / 0.08 h / 0 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 2 h / 0 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: lithium hydroxide monohydrate / N,N-dimethyl-formamide / Inert atmosphere

5.1: bis-[(trifluoroacetoxy)iodo]benzene; sodium hydrogencarbonate / 0.5 h / 0 °C / Inert atmosphere

With triethylsilane; n-butyllithium; lithium hydroxide monohydrate; boron trifluoride diethyl etherate; titanium tetrachloride; sodium hydrogencarbonate; bis-[(trifluoroacetoxy)iodo]benzene; zinc; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1039/c3ob27491h