diethyl 1-methyl-1-phenylthioethylphosphonate

Base Information

• Chemical Name: diethyl 1-methyl-1-phenylthioethylphosphonate
• CAS No.: 168129-74-6
• Molecular Formula: C₁₃H₂₁O₃PS
• Molecular Weight: 288.348
• Mol file: 168129-74-6.mol

Synonyms:

Chemical Property of diethyl 1-methyl-1-phenylthioethylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of diethyl 1-methyl-1-phenylthioethylphosphonate

There total 1 articles about diethyl 1-methyl-1-phenylthioethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl (1-(phenylthio)ethyl)phosphonate (55264-89-6) + methyl iodide (74-88-4) → diethyl 1-methyl-1-phenylthioethylphosphonate (168129-74-6)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) THF, -78 deg C, 2.) THF, -78 to 25 deg C, 2 h then 50 deg C, 20 min;

DOI:10.1016/0040-4020(95)00393-M

Reference yield: 86.0%

diethyl 1-methyl-1-phenylthioethylphosphonate (168129-74-6) → diethyl isopropylphosphonate (1538-69-8)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 1h; Heating;

upstream raw materials:

diethyl (1-(phenylthio)ethyl)phosphonate

methyl iodide

Downstream raw materials:

diethyl isopropylphosphonate