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diethyl 1-methyl-1-phenylthioethylphosphonate

Base Information
  • Chemical Name:diethyl 1-methyl-1-phenylthioethylphosphonate
  • CAS No.:168129-74-6
  • Molecular Formula:C13H21O3PS
  • Molecular Weight:288.348
  • Hs Code.:
diethyl 1-methyl-1-phenylthioethylphosphonate

Synonyms:

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of diethyl 1-methyl-1-phenylthioethylphosphonate
Chemical Property:
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Technology Process of diethyl 1-methyl-1-phenylthioethylphosphonate

There total 1 articles about diethyl 1-methyl-1-phenylthioethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With n-butyllithium; Yield given. Multistep reaction; 1.) THF, -78 deg C, 2.) THF, -78 to 25 deg C, 2 h then 50 deg C, 20 min;
DOI:10.1016/0040-4020(95)00393-M
Guidance literature:
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 1h; Heating;
upstream raw materials:

diethyl (1-(phenylthio)ethyl)phosphonate

methyl iodide

Downstream raw materials:

diethyl isopropylphosphonate

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