C₃₄H₄₂N₂O₄S

Base Information

Chemical Name:C₃₄H₄₂N₂O₄S
CAS No.:1428427-73-9
Molecular Formula:C₃₄H₄₂N₂O₄S
Molecular Weight:574.784
Hs Code.:

C<sub>34</sub>H<sub>42</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₃₄H₄₂N₂O₄S

Chemical Property:

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Technology Process of C₃₄H₄₂N₂O₄S

There total 15 articles about C₃₄H₄₂N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 6738-06-3
phenylethynylmagnesium bromide

: 1428427-69-3
C₂₆H₃₆N₂O₄S

: 1428427-71-7
C₃₄H₄₂N₂O₄S

: 1428427-73-9
C₃₄H₄₂N₂O₄S

Guidance literature:: In tetrahydrofuran; chlorobenzene; for 1h; diastereoselective reaction; Inert atmosphere; Reflux;
DOI:10.1021/ol400469w

Reference yield:

: 1428427-23-9
C₃₈H₄₃NO₄Si

: 1428427-71-7
C₃₄H₄₂N₂O₄S

: 1428427-73-9
C₃₄H₄₂N₂O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: lithium borohydride / ethanol / 4 h / Inert atmosphere

2: palladium 10% on activated carbon; ammonium formate / methanol / 12.5 h / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / Inert atmosphere

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / Inert atmosphere

5: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

6: copper(II) sulfate / toluene / 12 h / 20 °C / Inert atmosphere

7: tetrahydrofuran; chlorobenzene / 1 h / Inert atmosphere; Reflux

With lithium borohydride; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; ammonium formate; Dess-Martin periodane; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; chlorobenzene; toluene; 7: |Grignard Reaction;
DOI:10.1021/ol400469w

Reference yield:

: 1428427-25-1
C₃₈H₄₇NO₄Si

: 1428427-71-7
C₃₄H₄₂N₂O₄S

: 1428427-73-9
C₃₄H₄₂N₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: copper(II) sulfate / toluene / 12 h / 20 °C / Inert atmosphere

4: tetrahydrofuran; chlorobenzene / 1 h / Inert atmosphere; Reflux

With tetrabutyl ammonium fluoride; Dess-Martin periodane; copper(II) sulfate; In tetrahydrofuran; dichloromethane; chlorobenzene; toluene; 4: |Grignard Reaction;
DOI:10.1021/ol400469w