(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCH₃

Base Information

Chemical Name:(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCH₃
CAS No.:1351623-50-1
Molecular Formula:C₃₃H₄₉IrN₂O₂P₂
Molecular Weight:759.932
Hs Code.:

(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCH<sub>3</sub>

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Chemical Property of (2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCH₃

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Technology Process of (2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCH₃

There total 1 articles about (2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1351623-48-7
(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCl

: 2999-74-8
dimethylmagnesium

: 1351623-50-1
(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCH₃

Guidance literature:: In tetrahydrofuran; toluene; (Ar); mixt. of THF/toluene (0.1:4, v/v) was added to mixt. of iridium complex with Me2Mg, heated to 130°C for 3 d; evapd. in vac., extd. with toluene, concd., crystd. with pentane at -35°C, elem. anal.;
DOI:10.1039/c1nj20602h

Reference yield:

: tetrakis[3,5-bis(trifluoromethyl)phenyl]boric acid bis(diethyl ether) complex

: 1351623-50-1
(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)IrCH₃

: 1351623-54-5
[(2,6-bis(di-tert-butylphosphinito)-3,5-diphenylpyrazine)Ir(H)(CH₃)][B(3,5-(F₃C)2C₆H₃)4]

Guidance literature:: In further solvent(s); (Ar); NMR tube was charged with H(OEt2)2B(3,5-(CF3)2C6H3)4 and iridium compled, at 77°C CDCl2F was added, cooled to -100°C; detected by NMR;
DOI:10.1039/c1nj20602h