Technology Process of C16H10ClN3O
There total 7 articles about C16H10ClN3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iron; ammonium chloride;
In
ethanol; water;
DOI:10.1021/ja2058583
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / dimethyl sulfoxide / 110 °C
2: iron; ammonium chloride / ethanol; water
With
iron; potassium carbonate; ammonium chloride;
In
ethanol; water; dimethyl sulfoxide;
DOI:10.1021/ja2058583
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C
1.2: 1 h / 60 - 80 °C
2.1: boron tribromide / dichloromethane / 13 h / -78 - 20 °C / Inert atmosphere
3.1: bis(triphenylphosphine)palladium(II) dichloride; triethylamine / N,N-dimethyl-formamide / 3 h / 20 - 140 °C / Inert atmosphere
4.1: potassium carbonate / dimethyl sulfoxide / 110 °C
5.1: iron; ammonium chloride / ethanol; water
With
hydrogenchloride; bis(triphenylphosphine)palladium(II) dichloride; boron tribromide; iron; potassium carbonate; ammonium chloride; triethylamine; sodium nitrite;
In
ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
3.1: Heck reaction;
DOI:10.1021/ja2058583
