d₅-ethyl cyanophenylacetate

Base Information

Chemical Name:d₅-ethyl cyanophenylacetate
CAS No.:72793-43-2
Molecular Formula:C₁₁H₁₁NO₂
Molecular Weight:194.174
Hs Code.:

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Suppliers and Price of d₅-ethyl cyanophenylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of d₅-ethyl cyanophenylacetate

Chemical Property:

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Technology Process of d₅-ethyl cyanophenylacetate

There total 2 articles about d₅-ethyl cyanophenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 7379-67-1
d₅-iodobenzene

: 105-56-6
ethyl 2-cyanoacetate

: 72793-43-2
d₅-ethyl cyanophenylacetate

Guidance literature:: ethyl 2-cyanoacetate; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; Inert atmosphere; Schlenk technique;

d₅-iodobenzene; With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; mineral oil; at 0 ℃; for 5h; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1002/anie.201402008

Reference yield:

: 1076-43-3
benzene-d6

: 72793-43-2
d₅-ethyl cyanophenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate; n-butyllithium / hexane / 20 h / -78 - 0 °C / Inert atmosphere; Schlenk technique

1.2: 0.75 h / -78 °C / Inert atmosphere; Schlenk technique

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere; Schlenk technique

2.2: 5 h / 0 °C / Inert atmosphere; Schlenk technique; Reflux

With n-butyllithium; potassium tert-butylate; sodium hydride; In tetrahydrofuran; hexane; mineral oil;
DOI:10.1002/anie.201402008