β-p-Brombenzylnaphthalin

Base Information

• Chemical Name: β-p-Brombenzylnaphthalin
• CAS No.: 32891-97-7
• Molecular Formula: C₁₇H₁₃Br
• Molecular Weight: 297.194
• Mol file: 32891-97-7.mol

Synonyms:

Chemical Property of β-p-Brombenzylnaphthalin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of β-p-Brombenzylnaphthalin

There total 4 articles about β-p-Brombenzylnaphthalin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-Naphthalenemethanol (1592-38-7) + 4-Bromophenylboronic acid (5467-74-3) → β-p-Brombenzylnaphthalin (32891-97-7)

Guidance literature:

With alumina-grafted SBA-15 mesoporous silica; In 1,2-dichloro-ethane; at 80 ℃; for 6h; Catalytic behavior; Inert atmosphere;

DOI:10.1039/d0cy00471e

Reference yield:

naphthalene (91-20-3,71998-51-1,72931-45-4) + 4-bromobenzenemethanol (873-75-6) → 1-(4-bromobenzyl)naphthalene (32891-94-4) + β-p-Brombenzylnaphthalin (32891-97-7)

Guidance literature:

With ferroceniumboronic acid hexafluoroantimonate salt; In nitromethane; at 50 ℃; for 24h; Overall yield = 88 %; Overall yield = 130 mg; regioselective reaction;

DOI:10.1021/jacs.5b05076

Reference yield:

(4-bromophenyl)(naphthalene-2-yl)methanol (32891-96-6) → β-p-Brombenzylnaphthalin (32891-97-7)

Guidance literature:

With lithium aluminium tetrahydride; aluminium trichloride;

DOI:10.1039/j39710002264

upstream raw materials:

(4-bromophenyl)(naphthalene-2-yl)methanol

naphthalene

4-bromobenzenemethanol

2-Naphthalenemethanol