2--1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

Base Information

Chemical Name:2--1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole
CAS No.:101481-21-4
Molecular Formula:C₂₈H₂₆N₂OS₂
Molecular Weight:470.659
Hs Code.:

2-<bis(phenylthio)acetyl>-1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

Synonyms:

Suppliers and Price of 2--1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2--1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2--1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

There total 4 articles about 2--1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101481-19-0,101481-28-1
2-<(phenylsulfinyl)acetyl>-1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

: 101481-21-4
2--1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

Guidance literature:: With triethylamine; trifluoroacetic anhydride; at room temp. or at 80 deg C;
DOI:10.1016/S0040-4039(00)94994-3

Reference yield:

: 7031-27-8
(phenylthio)acetic acid chloride

: 101481-21-4
2--1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

Guidance literature:: Multi-step reaction with 3 steps

1: 1N NaOH / CH₂Cl₂

2: m-CPBA

3: TFAA, Et₃N / at room temp. or at 80 deg C

With sodium hydroxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane;
DOI:10.1016/S0040-4039(00)94994-3

Reference yield:

: 99552-97-3
1,2,3,4,5,6-hexahydro-1,5-methaneoazacino<4,3-b>indole

: 101481-21-4
2--1,2,3,4,5,6-hexahydro-1,5-methanoazocino<4,3-b>indole

Guidance literature:: Multi-step reaction with 3 steps

1: 1N NaOH / CH₂Cl₂

2: m-CPBA

3: TFAA, Et₃N / at room temp. or at 80 deg C

With sodium hydroxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane;
DOI:10.1016/S0040-4039(00)94994-3