tert-butyl (Z)-3-cyclohexylpropenoate

Base Information

Chemical Name:tert-butyl (Z)-3-cyclohexylpropenoate
CAS No.:87947-81-7
Molecular Formula:C₁₃H₂₂O₂
Molecular Weight:210.316
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (Z)-3-cyclohexylpropenoate

Chemical Property:

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Technology Process of tert-butyl (Z)-3-cyclohexylpropenoate

There total 5 articles about tert-butyl (Z)-3-cyclohexylpropenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27784-76-5
tert-butyl diethylphosphonoacetate

: 2043-61-0
cyclohexanecarbaldehyde

: 87947-81-7
tert-butyl (Z)-3-cyclohexylpropenoate

: 87947-80-6
tert-butyl (E)-3-cyclohexylpropenoate

Guidance literature:: tert-butyl diethylphosphonoacetate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

cyclohexanecarbaldehyde; In tetrahydrofuran; hexane; at -78 - 20 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol802212e

Reference yield:

: 695-12-5,25498-06-0
vinylcyclohexane

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 87947-81-7
tert-butyl (Z)-3-cyclohexylpropenoate

: 87947-80-6
tert-butyl (E)-3-cyclohexylpropenoate

Guidance literature:: With Mo(NC₆F₅)(CHCMe₂Ph)(2,5-dimethylpyrrolide)(2,6-dimesitylphenoxide); In acetonitrile; at 22 ℃; for 1h; under 100 Torr; Overall yield = 64 %; Overall yield = 11.1 mg; stereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201608087

Reference yield:

: 1048364-45-9
tert-butyl 2-[3,5-bis(trifluoromethyl)phenylsulfonyl]acetate

: 2043-61-0
cyclohexanecarbaldehyde

: 87947-81-7
tert-butyl (Z)-3-cyclohexylpropenoate

: 87947-80-6
tert-butyl (E)-3-cyclohexylpropenoate

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 18h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.200800041