C₂₈H₂₄N₂O₄

Base Information

Chemical Name:C₂₈H₂₄N₂O₄
CAS No.:90369-72-5
Molecular Formula:C₂₈H₂₄N₂O₄
Molecular Weight:452.51
Hs Code.:

C<sub>28</sub>H<sub>24</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₂₄N₂O₄

Chemical Property:

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Technology Process of C₂₈H₂₄N₂O₄

There total 6 articles about C₂₈H₂₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90369-65-6
2-hydroxy-2-(hydroxymethyl)-5-methylcyclohexanone

: 90369-72-5
C₂₈H₂₄N₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1.) 21 h, 70 deg C, 2.) additional PhCOCl, 24 h, 70 deg C

2: 1.) LiN(i-Pr)2, 2.) MoO₅*pyridine*HMPA (MoOPH) / from DB 2; 1.) THF, hexane, -70 deg C, 2.) -30 deg C

3: (CF₃CO)2O, Me₂SO, Et₃N / CH₂Cl₂ / 0.5 h / -70 °C

4: ethanol; acetic acid / Heating

With pyridine; oxodiperoxymolybdenumpyridine hexamethylphosphoric triamide complex; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; lithium diisopropyl amide; In ethanol; dichloromethane; acetic acid;
DOI:10.1021/jo00187a026

Reference yield:

: 90369-66-7,90369-67-8
2-hydroxy-2-(hydroxymethyl)-5-methylcyclohexanone dibenzoate

: 90369-72-5
C₂₈H₂₄N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LiN(i-Pr)2, 2.) MoO₅*pyridine*HMPA (MoOPH) / from DB 2; 1.) THF, hexane, -70 deg C, 2.) -30 deg C

2: (CF₃CO)2O, Me₂SO, Et₃N / CH₂Cl₂ / 0.5 h / -70 °C

3: ethanol; acetic acid / Heating

With oxodiperoxymolybdenumpyridine hexamethylphosphoric triamide complex; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; lithium diisopropyl amide; In ethanol; dichloromethane; acetic acid;
DOI:10.1021/jo00187a026

Reference yield:

: 98-88-4
benzoyl chloride

: 90369-72-5
C₂₈H₂₄N₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1.) 21 h, 70 deg C, 2.) additional PhCOCl, 24 h, 70 deg C

2: 1.) LiN(i-Pr)2, 2.) MoO₅*pyridine*HMPA (MoOPH) / from DB 2; 1.) THF, hexane, -70 deg C, 2.) -30 deg C

3: (CF₃CO)2O, Me₂SO, Et₃N / CH₂Cl₂ / 0.5 h / -70 °C

4: ethanol; acetic acid / Heating

With pyridine; oxodiperoxymolybdenumpyridine hexamethylphosphoric triamide complex; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; lithium diisopropyl amide; In ethanol; dichloromethane; acetic acid;
DOI:10.1021/jo00187a026