phenyl 2-(4-anisyl)-1-naphthoate

Base Information

Chemical Name:phenyl 2-(4-anisyl)-1-naphthoate
CAS No.:106520-93-8
Molecular Formula:C₂₄H₁₈O₃
Molecular Weight:354.405
Hs Code.:

Synonyms:

Suppliers and Price of phenyl 2-(4-anisyl)-1-naphthoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl 2-(4-anisyl)-1-naphthoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl 2-(4-anisyl)-1-naphthoate

There total 1 articles about phenyl 2-(4-anisyl)-1-naphthoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 106542-96-5
phenyl 2-methoxy-1-naphthoate

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 106520-93-8
phenyl 2-(4-anisyl)-1-naphthoate

Guidance literature:: In diethyl ether; benzene; 1.) reflux, 3 h, 2.) RT, overnight;
DOI:10.1021/jo00381a025

Reference yield:

: 106520-93-8
phenyl 2-(4-anisyl)-1-naphthoate

: 106521-01-1
4-hydroxybenzofluoranthene

Guidance literature:: Multi-step reaction with 11 steps

1: 100 percent / methanesulfonic acid / 1.5 h / Ambient temperature

2: 59 percent / zinc amalgam, conc. HCl / toluene; acetic acid / 27 h / Heating

3: 1.) n-BuLi / 1.) ether, hexane, -30 deg C, 1 h, 2.) ether, hexane, from -30 deg C to RT

4: 69 percent / conc,. H₂SO₄ / benzene / 20 h / Heating

5: 96 percent / 10 N NaOH / pyridine / 3 h / Ambient temperature

6: 97 percent / 10 N NaOH / ethanol / 17 h / Heating

7: 70 percent / methanesulfonic acid / 19 h / Ambient temperature

8: NaBH₄ / methanol / 0.67 h / Ambient temperature

9: p-toluenesulfonic acid / benzene / 2 h / Heating

10: 100 percent / 1-methylnaphthalene / benzene / 7 h / Heating

11: 96 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 1 h, 2.) RT, 2 h

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; amalgamated zinc; n-butyllithium; methanesulfonic acid; sulfuric acid; boron tribromide; toluene-4-sulfonic acid; 1-Methylnaphthalene; In pyridine; methanol; ethanol; dichloromethane; acetic acid; toluene; benzene;
DOI:10.1021/jo00381a025

Reference yield:

: 106520-93-8
phenyl 2-(4-anisyl)-1-naphthoate

: 106521-02-2
benzofluoranthene-4,5-dione

Guidance literature:: Multi-step reaction with 12 steps

1: 100 percent / methanesulfonic acid / 1.5 h / Ambient temperature

2: 59 percent / zinc amalgam, conc. HCl / toluene; acetic acid / 27 h / Heating

3: 1.) n-BuLi / 1.) ether, hexane, -30 deg C, 1 h, 2.) ether, hexane, from -30 deg C to RT

4: 69 percent / conc,. H₂SO₄ / benzene / 20 h / Heating

5: 96 percent / 10 N NaOH / pyridine / 3 h / Ambient temperature

6: 97 percent / 10 N NaOH / ethanol / 17 h / Heating

7: 70 percent / methanesulfonic acid / 19 h / Ambient temperature

8: NaBH₄ / methanol / 0.67 h / Ambient temperature

9: p-toluenesulfonic acid / benzene / 2 h / Heating

10: 100 percent / 1-methylnaphthalene / benzene / 7 h / Heating

11: 96 percent / BBr₃ / CH₂Cl₂ / 1.) -78 deg C, 1 h, 2.) RT, 2 h

12: 94 percent / Adogen 464, potassium nitrosodisulfonate, 1/6 M KH₂PO₄ / benzene; H₂O / 2 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; potassium dihydrogenphosphate; amalgamated zinc; n-butyllithium; adogen 464; methanesulfonic acid; potassiuim nitrosodisulfonate; sulfuric acid; boron tribromide; toluene-4-sulfonic acid; 1-Methylnaphthalene; In pyridine; methanol; ethanol; dichloromethane; water; acetic acid; toluene; benzene;
DOI:10.1021/jo00381a025