3-nitro-1,5-di-p-phenetolformazan

Base Information

Chemical Name:3-nitro-1,5-di-p-phenetolformazan
CAS No.:28952-15-0
Molecular Formula:C₁₇H₁₉N₅O₄
Molecular Weight:357.369
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-nitro-1,5-di-p-phenetolformazan

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Technology Process of 3-nitro-1,5-di-p-phenetolformazan

There total 1 articles about 3-nitro-1,5-di-p-phenetolformazan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19262-82-9
4-ethoxybenzenediazonium

: 127-09-3
sodium acetate

: 28952-15-0
3-nitro-1,5-di-p-phenetolformazan

Guidance literature:: With acetic acid; anschliessend mit Nitromethan;

Reference yield:

: 28952-15-0
3-nitro-1,5-di-p-phenetolformazan

: palladium dichloride

: 171202-02-1
bis(3-nitro-1,5-dip-phenitylformazan)Pd(II)

Guidance literature:: With potassium nitrite; In water; acetone; heating, stirring, refluxing (6 h); evapn., crystn. (chloroform-hexane), chromatography (hexane, benzene-hexane, benzene), recrystn. (benzene-hexane); elem. anal.;

Reference yield:

: rhodium(III) chloride trihydrate

: 28952-15-0
3-nitro-1,5-di-p-phenetolformazan

: tris(3-nitro-1,5-di-p-phenetolformazanato)rhodium(III)

Guidance literature:: With sodium acetate; In methanol; reflux (water bath), CH3COONa addn., pH=6-7, reflux (3-4 h), solvent evapn. (water bath); residue washing (water), chromatography (chloroform), concn., recrystn. (chloroform-hexane); elem. anal.;