C₁₅H₂₀N₂O₃

Base Information

Chemical Name:C₁₅H₂₀N₂O₃
CAS No.:1262949-02-9
Molecular Formula:C₁₅H₂₀N₂O₃
Molecular Weight:276.335
Hs Code.:

C<sub>15</sub>H<sub>20</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₀N₂O₃

Chemical Property:

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Technology Process of C₁₅H₂₀N₂O₃

There total 5 articles about C₁₅H₂₀N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 1262949-02-9
C₁₅H₂₀N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: Jones reagent / diethyl ether / 0 - 20 °C / Inert atmosphere

2.1: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C / Inert atmosphere

3.1: 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; copper diacetate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

4.1: triphenylphosphine / tetrahydrofuran / 4 h / 50 °C / Inert atmosphere

4.2: 16 h / 20 °C / Inert atmosphere

5.1: tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With Jones reagent; hydroxylamine hydrochloride; copper diacetate; sodium acetate; triphenylphosphine; 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In tetrahydrofuran; diethyl ether; ethanol; water; N,N-dimethyl-formamide; 4.1: |Staudinger Azide Reduction;
DOI:10.1021/ol403687k

Reference yield:

: 100-52-7
benzaldehyde

: 1262949-02-9
C₁₅H₂₀N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: zinc / tetrahydrofuran / 0 °C / Inert atmosphere

2.1: Jones reagent / diethyl ether / 0 - 20 °C / Inert atmosphere

3.1: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C / Inert atmosphere

4.1: 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; copper diacetate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

5.1: triphenylphosphine / tetrahydrofuran / 4 h / 50 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

6.1: tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With Jones reagent; hydroxylamine hydrochloride; copper diacetate; sodium acetate; triphenylphosphine; 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; zinc; In tetrahydrofuran; diethyl ether; ethanol; water; N,N-dimethyl-formamide; 5.1: |Staudinger Azide Reduction;
DOI:10.1021/ol403687k

Reference yield:

: 6249-80-5
1-phenylbut-3-en-1-one

: 1262949-02-9
C₁₅H₂₀N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C / Inert atmosphere

2.1: 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; copper diacetate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

3.1: triphenylphosphine / tetrahydrofuran / 4 h / 50 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

4.1: tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

With hydroxylamine hydrochloride; copper diacetate; sodium acetate; triphenylphosphine; 1-azido-1λ³-benzo[d][1,2]iodaoxol-3(1H)-one; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; 3.1: |Staudinger Azide Reduction;
DOI:10.1021/ol403687k