Technology Process of 2-[2-(2-Methyl-oxiranylmethoxy)-phenoxymethyl]-1,4,7,10-tetraoxa-cyclododecane
There total 5 articles about 2-[2-(2-Methyl-oxiranylmethoxy)-phenoxymethyl]-1,4,7,10-tetraoxa-cyclododecane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 40percent aqueous NaOH / Heating
2: H2O / HClO4 / 80 °C
3: 16 percent / lithium cation
4: m-chloroperoxybenzoic acid, NaHCO3 / CHCl3 / 15 h
With
sodium hydroxide; water; lithium cation; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
perchloric acid;
In
chloroform;
DOI:10.1021/jo00187a024
- Guidance literature:
-
Multi-step reaction with 3 steps
1: H2O / HClO4 / 80 °C
2: 16 percent / lithium cation
3: m-chloroperoxybenzoic acid, NaHCO3 / CHCl3 / 15 h
With
water; lithium cation; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
perchloric acid;
In
chloroform;
DOI:10.1021/jo00187a024
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 50 percent / K2CO3, KI / acetone / 24 h / Heating
2: 40percent aqueous NaOH / Heating
3: H2O / HClO4 / 80 °C
4: 16 percent / lithium cation
5: m-chloroperoxybenzoic acid, NaHCO3 / CHCl3 / 15 h
With
sodium hydroxide; water; lithium cation; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium iodide;
perchloric acid;
In
chloroform; acetone;
DOI:10.1021/jo00187a024
