1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrole

Base Information

Chemical Name:1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrole
CAS No.:161181-93-7
Molecular Formula:C₂₀H₂₂N₂O₄
Molecular Weight:354.406
Hs Code.:

1-<4-(tert-butyloxycarbonyl)phenyl>-3-<cyano(ethoxycarbonyl)methyl>pyrrole

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Chemical Property of 1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrole

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Technology Process of 1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrole

There total 3 articles about 1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.9%

: 94930-27-5
1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrolidinone

: 105-56-6
ethyl 2-cyanoacetate

: 161181-93-7
1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrole

Guidance literature:: With ammonium acetate; acetic acid; In benzene; for 6h; Heating;
DOI:10.1002/jhet.5570310522

Reference yield:

: 58656-98-7
tert-butyl 4-fluorobenzoate

: 161181-93-7
1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / K₂CO₃ / dimethylsulfoxide / 6.5 h / 120 - 125 °C

2: 73 percent / N,N-dicyclohexylcarbodiimide, pyridine, trifluoroacetic acid, DMSO / benzene / 18 h / 5 - 20 °C

3: 4.9 percent / ammonium acetate, gl. AcOH / benzene / 6 h / Heating

With pyridine; ammonium acetate; potassium carbonate; acetic acid; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dimethyl sulfoxide; benzene;
DOI:10.1002/jhet.5570310522

Reference yield:

: 94930-28-6
N-<4'-(tert-butoxycarbonyl)phenyl>-3-pyrrolidinol

: 161181-93-7
1-<4-(tert-butyloxycarbonyl)phenyl>-3-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / N,N-dicyclohexylcarbodiimide, pyridine, trifluoroacetic acid, DMSO / benzene / 18 h / 5 - 20 °C

2: 4.9 percent / ammonium acetate, gl. AcOH / benzene / 6 h / Heating

With pyridine; ammonium acetate; acetic acid; dimethyl sulfoxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In benzene;
DOI:10.1002/jhet.5570310522