C₃₃H₃₆FN₇O₅S

Base Information

• Chemical Name: C₃₃H₃₆FN₇O₅S
• CAS No.: 1344734-52-6
• Molecular Formula: C₃₃H₃₆FN₇O₅S
• Molecular Weight: 661.757
• Mol file: 1344734-52-6.mol

Synonyms:

Chemical Property of C₃₃H₃₆FN₇O₅S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₃₆FN₇O₅S

There total 11 articles about C₃₃H₃₆FN₇O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-{4-[(5-formyl-6-methyl-2-pyridinyl)oxy]-3-methylphenyl}methanesulfonamide (1150103-15-3) + C18H20FN5O2*2ClH → C33H36FN7O5S (1344734-52-6)

Guidance literature:

With sodium tris(acetoxy)borohydride; triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmcl.2011.08.080

Reference yield:

5-isocyanatopicolinonitrile (125117-98-8) → C33H36FN7O5S (1344734-52-6)

Guidance literature:

Multi-step reaction with 4 steps

1: dichloromethane / 24 h

2: urea hydrogen peroxide adduct; potassium carbonate / water; acetone / 24 h / 20 °C

3: hydrogenchloride / 1,4-dioxane

4: sodium tris(acetoxy)borohydride; triethylamine / dichloromethane / 20 °C

With hydrogenchloride; urea hydrogen peroxide adduct; sodium tris(acetoxy)borohydride; potassium carbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; acetone;

DOI:10.1016/j.bmcl.2011.08.080

Reference yield:

tert-butyl 4-((3-fluorophenyl)amino)piperidine-1-carboxylate (679409-18-8) → C33H36FN7O5S (1344734-52-6)

Guidance literature:

Multi-step reaction with 4 steps

1: dichloromethane / 24 h

2: urea hydrogen peroxide adduct; potassium carbonate / water; acetone / 24 h / 20 °C

3: hydrogenchloride / 1,4-dioxane

4: sodium tris(acetoxy)borohydride; triethylamine / dichloromethane / 20 °C

With hydrogenchloride; urea hydrogen peroxide adduct; sodium tris(acetoxy)borohydride; potassium carbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; acetone;

DOI:10.1016/j.bmcl.2011.08.080

upstream raw materials:

5-isocyanatopicolinonitrile

tert-butyl 4-((3-fluorophenyl)amino)piperidine-1-carboxylate

N-(4-hydroxy-3-methylphenyl)methanesulfonamide

meta-fluoroaniline