C₅₈H₆₈N₂O₁₅

Base Information

Chemical Name:C₅₈H₆₈N₂O₁₅
CAS No.:187142-86-5
Molecular Formula:C₅₈H₆₈N₂O₁₅
Molecular Weight:1033.18
Hs Code.:

C<sub>58</sub>H<sub>68</sub>N<sub>2</sub>O<sub>15</sub>

Synonyms:

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Chemical Property of C₅₈H₆₈N₂O₁₅

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Technology Process of C₅₈H₆₈N₂O₁₅

There total 10 articles about C₅₈H₆₈N₂O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33639-77-9
perbenzyl fucosyl bromide

: 187142-86-5
C₅₈H₆₈N₂O₁₅

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / Et₄NBr, mol. sieves 4A / CH₂Cl₂; dimethylformamide / 144 h

2: hydrazine hydrate / ethanol; toluene / 12 h / Heating

3: methanol / 4 h / Ambient temperature

With 4 A molecular sieve; tetraethylammonium bromide; hydrazine hydrate; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0968-0896(96)00182-4

Reference yield:

: 81927-56-2
methyl 4,6-O-benzylidene-2-deoxy-2-phthalimide-β-D-glucopyranoside

: 187142-86-5
C₅₈H₆₈N₂O₁₅

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaBH₃CN, mol. sieves 3A, 2.) HCl / 1.) THF, RT, 30 min, 2.) THF, ether, RT, 3 h

2: 81 percent / mol. sieves 4A, NIS, AgOTf / CH₂Cl₂; toluene / 0.33 h / -45 °C

3: 65 percent / Et₄NBr, mol. sieves 4A / CH₂Cl₂; dimethylformamide / 144 h

4: hydrazine hydrate / ethanol; toluene / 12 h / Heating

5: methanol / 4 h / Ambient temperature

With hydrogenchloride; N-iodo-succinimide; 3 A molecular sieve; 4 A molecular sieve; tetraethylammonium bromide; silver trifluoromethanesulfonate; sodium cyanoborohydride; hydrazine hydrate; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0968-0896(96)00182-4

Reference yield:

: 100-52-7
benzaldehyde

: 187142-86-5
C₅₈H₆₈N₂O₁₅

Guidance literature:: Multi-step reaction with 6 steps

1: 96percent aq. HCO₂H / 3 h / Ambient temperature

2: 99 percent / pyridine / CH₂Cl₂ / 0.08 h

3: 81 percent / mol. sieves 4A, NIS, AgOTf / CH₂Cl₂; toluene / 0.33 h / -45 °C

4: 65 percent / Et₄NBr, mol. sieves 4A / CH₂Cl₂; dimethylformamide / 144 h

5: hydrazine hydrate / ethanol; toluene / 12 h / Heating

6: methanol / 4 h / Ambient temperature

With pyridine; N-iodo-succinimide; formic acid; 4 A molecular sieve; tetraethylammonium bromide; silver trifluoromethanesulfonate; hydrazine hydrate; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0968-0896(96)00182-4