Technology Process of 3,9-Dibenzyladenine Perchlorate
There total 6 articles about 3,9-Dibenzyladenine Perchlorate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 94 percent / anhydrous K2CO3 / dimethylformamide / 5 h / Ambient temperature
2: 1.) H2, 1N aqueous HCl, 2.) 70percent aqueous HClO4 / 1.) room temperature. 3 h, 2.) EtOH, reflux, 8 h,
With
hydrogenchloride; perchloric acid; hydrogen; potassium carbonate;
In
N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.1504
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 94 percent / anhydrous K2CO3 / dimethylformamide / 5 h / Ambient temperature
2: 1.) H2, 1N aqueous HCl, 2.) 70percent aqueous HClO4 / 1.) room temperature. 3 h, 2.) EtOH, reflux, 8 h,
With
hydrogenchloride; perchloric acid; hydrogen; potassium carbonate;
In
N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.1504
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84 percent / 10percent aqueous Na2CO3 / 60 °C
2: 94 percent / anhydrous K2CO3 / dimethylformamide / 5 h / Ambient temperature
3: 1.) H2, 1N aqueous HCl, 2.) 70percent aqueous HClO4 / 1.) room temperature. 3 h, 2.) EtOH, reflux, 8 h,
With
hydrogenchloride; perchloric acid; hydrogen; sodium carbonate; potassium carbonate;
In
N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.1504