Technology Process of C17H26O5
There total 6 articles about C17H26O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sulfuric acid / N,N-dimethyl-formamide / 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide
2.2: 4 h / 20 °C
3.1: hydrogenchloride; water / methanol / 4 h / 20 °C
4.1: sodium periodate / ethanol; water; methanol / 3 h / 20 °C
5.1: sodium tetrahydroborate / ethanol / 2 h / 20 °C
6.1: triethylsilane; titanium tetrachloride / dichloromethane / 0.08 h / -78 °C / Inert atmosphere
With
hydrogenchloride; triethylsilane; sodium tetrahydroborate; sodium periodate; sulfuric acid; water; titanium tetrachloride; sodium hydride;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:org/10.1016/j.tetlet.2012.08.143
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / ethanol / 2 h / 20 °C
2: triethylsilane; titanium tetrachloride / dichloromethane / 0.08 h / -78 °C / Inert atmosphere
With
triethylsilane; sodium tetrahydroborate; titanium tetrachloride;
In
ethanol; dichloromethane;
DOI:org/10.1016/j.tetlet.2012.08.143
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / N,N-dimethyl-formamide
1.2: 4 h / 20 °C
2.1: hydrogenchloride; water / methanol / 4 h / 20 °C
3.1: sodium periodate / ethanol; water; methanol / 3 h / 20 °C
4.1: sodium tetrahydroborate / ethanol / 2 h / 20 °C
5.1: triethylsilane; titanium tetrachloride / dichloromethane / 0.08 h / -78 °C / Inert atmosphere
With
hydrogenchloride; triethylsilane; sodium tetrahydroborate; sodium periodate; water; titanium tetrachloride; sodium hydride;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:org/10.1016/j.tetlet.2012.08.143