C₁₆⁽¹³⁾CH₁₇N₅O₄

Base Information

Chemical Name:C₁₆⁽¹³⁾CH₁₇N₅O₄
CAS No.:144963-56-4
Molecular Formula:C₁₇H₁₇N₅O₄
Molecular Weight:356.342
Hs Code.:

C<sub>16</sub><sup>(13)</sup>CH<sub>17</sub>N<sub>5</sub>O<sub>4</sub>

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Chemical Property of C₁₆⁽¹³⁾CH₁₇N₅O₄

Chemical Property:

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Technology Process of C₁₆⁽¹³⁾CH₁₇N₅O₄

There total 11 articles about C₁₆⁽¹³⁾CH₁₇N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈⁽¹³⁾CH₄₃N₅O₅Si₂

: 144963-56-4
C₁₆⁽¹³⁾CH₁₇N₅O₄

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 75 ℃; Yield given;
DOI:10.1016/S0040-4039(00)79089-7

Reference yield:

: <1-(13)C>-D-Ribose

: 144963-56-4
C₁₆⁽¹³⁾CH₁₇N₅O₄

Guidance literature:: Multi-step reaction with 10 steps

1: H₂SO₄ / 0 °C

2: pyridine / 0 °C

3: 95 percent / BF₃*Et₂O / CH₂Cl₂ / 1 h / 0 °C

4: 95 percent / m-CPBA, NaHCO₃ / CH₂Cl₂ / 1 h / 0 °C

5: 1) TMSOTf / 1) 1,2-dichloroethane, 0.5 h, r.t., 2) 1 min

6: 2M NaOH, pyridine / methanol / 0.08 h / 0 °C

7: pyridine / Ambient temperature

8: DMAP / acetonitrile / Ambient temperature

9: Bu₃SnH, AIBN / toluene / Heating

10: Bu₄NF / tetrahydrofuran / 75 °C

With pyridine; dmap; sodium hydroxide; 2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; sulfuric acid; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1016/S0040-4039(00)79089-7

Reference yield:

: 335595-58-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-<1-13C>ribofuranoside

: 144963-56-4
C₁₆⁽¹³⁾CH₁₇N₅O₄

Guidance literature:: Multi-step reaction with 8 steps

1: BF₃*Et₂O / CH₂Cl₂

2: 95 percent / m-CPBA, NaHCO₃ / CH₂Cl₂ / 1 h / 0 °C

3: 1) TMSOTf / 1) 1,2-dichloroethane, 0.5 h, r.t., 2) 1 min

4: 2M NaOH, pyridine / methanol / 0.08 h / 0 °C

5: pyridine / Ambient temperature

6: DMAP / acetonitrile / Ambient temperature

7: Bu₃SnH, AIBN / toluene / Heating

8: Bu₄NF / tetrahydrofuran / 75 °C

With pyridine; dmap; sodium hydroxide; 2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1016/S0040-4039(00)79089-7