C₂₈H₂₄Cl₂O₂

Base Information

Chemical Name:C₂₈H₂₄Cl₂O₂
CAS No.:103561-01-9
Molecular Formula:C₂₈H₂₄Cl₂O₂
Molecular Weight:463.403
Hs Code.:

C<sub>28</sub>H<sub>24</sub>Cl<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₈H₂₄Cl₂O₂

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Technology Process of C₂₈H₂₄Cl₂O₂

There total 10 articles about C₂₈H₂₄Cl₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 619-42-1
4-methoxycarbonylphenyl bromide

: 103561-01-9
C₂₈H₂₄Cl₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / CuCl / pyridine / 20 h / Heating

2: 91 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄

3: 62 percent / Zn, PdCl₂(PPh₃)2 / 1,2-dimethoxy-ethane / 21 h / Ambient temperature

4: 83 percent / Zn-Hg/HCl

5: 92 percent / LiAlH₄

6: 70 percent / SOCl₂

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; lithium aluminium tetrahydride; thionyl chloride; Perbenzoic acid; mercury; copper(l) chloride; zinc; In pyridine; tetrachloromethane; 1,2-dimethoxyethane;
DOI:10.1016/S0040-4039(00)94949-9

Reference yield:

: 24856-58-4
1,1-dimethoxy-1-(4-bromophenyl)methane

: 103561-01-9
C₂₈H₂₄Cl₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) pyridine, 20 h, reflux, 2.) acid hydrolysis

2: 1.) Jones oxidation, 2.) oxalyl chloride

3: 62 percent / Zn, PdCl₂(PPh₃)2 / 1,2-dimethoxy-ethane / 21 h / Ambient temperature

4: 83 percent / Zn-Hg/HCl

5: 92 percent / LiAlH₄

6: 70 percent / SOCl₂

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; lithium aluminium tetrahydride; thionyl chloride; oxalyl dichloride; mercury; zinc; In 1,2-dimethoxyethane;
DOI:10.1016/S0040-4039(00)94949-9

Reference yield:

: 3019-89-4
sodium 3-methylphenoxide

: 103561-01-9
C₂₈H₂₄Cl₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / CuCl / pyridine / 20 h / Heating

2: 91 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄

3: 62 percent / Zn, PdCl₂(PPh₃)2 / 1,2-dimethoxy-ethane / 21 h / Ambient temperature

4: 83 percent / Zn-Hg/HCl

5: 92 percent / LiAlH₄

6: 70 percent / SOCl₂

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; lithium aluminium tetrahydride; thionyl chloride; Perbenzoic acid; mercury; copper(l) chloride; zinc; In pyridine; tetrachloromethane; 1,2-dimethoxyethane;
DOI:10.1016/S0040-4039(00)94949-9