1-(2-((1-(ethoxycarbonyloxy)cyclohexyl methoxycarbonylmethyl)carbamoyl)-3-phenyl propyldisulfanylmethyl)-3-methylsulfanylpropyl ammonium trifluoroacetate

Base Information

Chemical Name:1-(2-((1-(ethoxycarbonyloxy)cyclohexyl methoxycarbonylmethyl)carbamoyl)-3-phenyl propyldisulfanylmethyl)-3-methylsulfanylpropyl ammonium trifluoroacetate
CAS No.:1098011-54-1
Molecular Formula:C₂HF₃O₂*C₂₇H₄₂N₂O₆S₃
Molecular Weight:700.862
Hs Code.:

1-(2-((1-(ethoxycarbonyloxy)cyclohexyl methoxycarbonylmethyl)carbamoyl)-3-phenyl propyldisulfanylmethyl)-3-methylsulfanylpropyl ammonium trifluoroacetate

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Chemical Property of 1-(2-((1-(ethoxycarbonyloxy)cyclohexyl methoxycarbonylmethyl)carbamoyl)-3-phenyl propyldisulfanylmethyl)-3-methylsulfanylpropyl ammonium trifluoroacetate

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Technology Process of 1-(2-((1-(ethoxycarbonyloxy)cyclohexyl methoxycarbonylmethyl)carbamoyl)-3-phenyl propyldisulfanylmethyl)-3-methylsulfanylpropyl ammonium trifluoroacetate

There total 14 articles about 1-(2-((1-(ethoxycarbonyloxy)cyclohexyl methoxycarbonylmethyl)carbamoyl)-3-phenyl propyldisulfanylmethyl)-3-methylsulfanylpropyl ammonium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.3%

: 1098011-54-1
1-(2-((1-(ethoxycarbonyloxy)cyclohexyl methoxycarbonylmethyl)carbamoyl)-3-phenyl propyldisulfanylmethyl)-3-methylsulfanylpropyl ammonium trifluoroacetate

Guidance literature:

Reference yield:

: 1616274-77-1
C₃₂H₅₀N₂O₈S₃

: 76-05-1
trifluoroacetic acid

: 1098011-54-1
1-(2-((1-(ethoxycarbonyloxy)cyclohexyl methoxycarbonylmethyl)carbamoyl)-3-phenyl propyldisulfanylmethyl)-3-methylsulfanylpropyl ammonium trifluoroacetate

Guidance literature:: C₃₂H₅₀N₂O₈S₃; With formic acid; at 20 ℃; for 1h;

trifluoroacetic acid; In water; acetonitrile;
DOI:10.1021/jm500602h

Reference yield:

: 102246-52-6
C₁₀H₁₇ClO₃

: 1098011-54-1
1-(2-((1-(ethoxycarbonyloxy)cyclohexyl methoxycarbonylmethyl)carbamoyl)-3-phenyl propyldisulfanylmethyl)-3-methylsulfanylpropyl ammonium trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / ethyl acetate / 0.25 h / 20 °C

1.2: 12 h / Reflux

2.1: dichloromethane / 2 h / 0 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0.33 h / 20 °C

4.1: formic acid / 1 h / 20 °C

With formic acid; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm500602h