Technology Process of C27H32N4O8Si
There total 9 articles about C27H32N4O8Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: DAST / CH2Cl2 / 0.17 h
1.2: DBU; BrCCl3 / CH2Cl2 / 4 h / 20 °C
2.1: HF-pyridine / tetrahydrofuran / 10 h / 20 °C
3.1: H2 / Pd/C / methanol / 8 h / 20 °C
4.1: DMAP; EDCI / dimethylformamide / 18 h / 20 °C
5.1: DAST / CH2Cl2 / 0.17 h
5.2: DBU; BrCCl3 / CH2Cl2 / 4 h / 20 °C
With
dmap; hydrogen; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4,4'-diaminostilbene-2,2'-disulfonic acid;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/com-06-s(o)38
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: HF-pyridine / tetrahydrofuran / 10 h / 20 °C
2.1: H2 / Pd/C / methanol / 8 h / 20 °C
3.1: DMAP; EDCI / dimethylformamide / 18 h / 20 °C
4.1: DAST / CH2Cl2 / 0.17 h
4.2: DBU; BrCCl3 / CH2Cl2 / 4 h / 20 °C
With
dmap; hydrogen; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4,4'-diaminostilbene-2,2'-disulfonic acid;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/com-06-s(o)38
- Guidance literature:
-
C27H36N4O9Si;
With
4,4'-diaminostilbene-2,2'-disulfonic acid;
In
dichloromethane;
for 0.166667h;
With
Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane;
at 20 ℃;
for 4h;
Further stages.;
DOI:10.3987/com-06-s(o)38
