C₃₀H₃₉NO₃Si

Base Information Edit

Chemical Name:C₃₀H₃₉NO₃Si
CAS No.:1452372-78-9
Molecular Formula:C₃₀H₃₉NO₃Si
Molecular Weight:489.73
Hs Code.:
Mol file:1452372-78-9.mol

C<sub>30</sub>H<sub>39</sub>NO<sub>3</sub>Si

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Chemical Property of C₃₀H₃₉NO₃Si Edit

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Technology Process of C₃₀H₃₉NO₃Si

There total 2 articles about C₃₀H₃₉NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1452372-75-6
4-hydroxy-N-((1S,2S)-1-hydroxy-1-phenylpropan-2-yl)-N-methylbutanamide

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1452372-78-9
C₃₀H₃₉NO₃Si

Guidance literature:: With dmap; triethylamine; In dichloromethane;
DOI:10.3762/bjoc.9.132

Reference yield:

: 90-82-4,7009-81-6,90-83-5,6912-63-6
pseudoephedrine

: 1452372-78-9
C₃₀H₃₉NO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; lithium chloride / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 - 20 °C / Inert atmosphere

2.1: dmap; triethylamine / dichloromethane

With dmap; n-butyllithium; triethylamine; lithium chloride; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.3762/bjoc.9.132

Reference yield:

: 1452372-78-9
C₃₀H₃₉NO₃Si

: 1452372-93-8
(S,E)-tert-butyl((3-((naphthalen-2-ylmethoxy)methyl)-7-(trityloxy)hept-5-en-1-yl)oxy)diphenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: lithium chloride; lithium diisopropyl amide / tetrahydrofuran

2: lithium amidotrihydridoborate / tetrahydrofuran / 0 - 20 °C

3: sodium hydride; tetra-(n-butyl)ammonium iodide; 1H-imidazole / tetrahydrofuran / 0 °C

With 1H-imidazole; lithium amidotrihydridoborate; tetra-(n-butyl)ammonium iodide; sodium hydride; lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; 1: |Myers's Alkylation;
DOI:10.3762/bjoc.9.132