C₃₁H₃₁N₅O₂

Base Information

Chemical Name:C₃₁H₃₁N₅O₂
CAS No.:1380115-27-4
Molecular Formula:C₃₁H₃₁N₅O₂
Molecular Weight:505.619
Hs Code.:

C<sub>31</sub>H<sub>31</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₃₁N₅O₂

Chemical Property:

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Technology Process of C₃₁H₃₁N₅O₂

There total 8 articles about C₃₁H₃₁N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: (2S,2'S)-N,N'-(pyridine-2,6-diyl)bis(2-amino-3-phenylpropanamide)

: 626-15-3
1,3-bis-(bromomethyl)benzene

: 1380115-27-4
C₃₁H₃₁N₅O₂

Guidance literature:: With tetrabutyl-ammonium chloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; for 24h; Reflux; Inert atmosphere;
DOI:10.1002/chem.201101416

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 1380115-27-4
C₃₁H₃₁N₅O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / tetrahydrofuran / 0.5 h / -5 °C / Inert atmosphere

2.1: tetrahydrofuran / 1.25 h / -5 °C / Inert atmosphere

3.1: hydrogen bromide; acetic acid / 1 h / Inert atmosphere

3.2: pH 12 - 13

4.1: tetrabutyl-ammonium chloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / Reflux; Inert atmosphere

With tetrabutyl-ammonium chloride; hydrogen bromide; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.201101416

Reference yield:

: 109453-49-8
(C₈H₇O₂)(NHCHCOO)(CH₂C₆H₅)(CO₂C₂H₅)

: 1380115-27-4
C₃₁H₃₁N₅O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 1.25 h / -5 °C / Inert atmosphere

2.1: hydrogen bromide; acetic acid / 1 h / Inert atmosphere

2.2: pH 12 - 13

3.1: tetrabutyl-ammonium chloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / Reflux; Inert atmosphere

With tetrabutyl-ammonium chloride; hydrogen bromide; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.201101416