N-[3-(dimethylamino)propyl]-4-{[(4-{[(4-{[imino(3-methoxyphenyl)methyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrole-2-carboxamide

Base Information

Chemical Name:N-[3-(dimethylamino)propyl]-4-{[(4-{[(4-{[imino(3-methoxyphenyl)methyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrole-2-carboxamide
CAS No.:1000276-89-0
Molecular Formula:C₃₁H₃₉N₉O₄
Molecular Weight:601.709
Hs Code.:

N-[3-(dimethylamino)propyl]-4-{[(4-{[(4-{[imino(3-methoxyphenyl)methyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrole-2-carboxamide

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Chemical Property of N-[3-(dimethylamino)propyl]-4-{[(4-{[(4-{[imino(3-methoxyphenyl)methyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrole-2-carboxamide

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Technology Process of N-[3-(dimethylamino)propyl]-4-{[(4-{[(4-{[imino(3-methoxyphenyl)methyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrole-2-carboxamide

There total 8 articles about N-[3-(dimethylamino)propyl]-4-{[(4-{[(4-{[imino(3-methoxyphenyl)methyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrole-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 154142-59-3
methyl 3-methoxybenzenecarbimidothioate hydroiodide

: 78486-18-7
3-(1-methyl-4-(1-methyl-4-(1-methyl-4-aminopyrrole-2-carboxamido)pyrrole-2-carboxamido)pyrrole-2-carboxamido)dimethylaminopropane

: 1000276-89-0
N-[3-(dimethylamino)propyl]-4-{[(4-{[(4-{[imino(3-methoxyphenyl)methyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: In methanol; at 20 ℃; for 48h;
DOI:10.1021/jm070831g

Reference yield:

: 28494-51-1
1-methyl-4-nitro-1H-pyrrole-2-carbonyl chloride

: 1000276-89-0
N-[3-(dimethylamino)propyl]-4-{[(4-{[(4-{[imino(3-methoxyphenyl)methyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol

With palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane;
DOI:10.1016/j.ejmech.2017.05.039

Reference yield:

: 13138-78-8
1-methyl-4-nitro-pyrrol-2-carboxylic acid

: 1000276-89-0
N-[3-(dimethylamino)propyl]-4-{[(4-{[(4-{[imino(3-methoxyphenyl)methyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrol-2-yl)carbonyl]amino}-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / dichloromethane / 2 h / Reflux

2: triethylamine / dichloromethane / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol

With thionyl chloride; palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane;
DOI:10.1016/j.ejmech.2017.05.039