(hydroxydimesitylsilyl)dimesitylgermane

Base Information

Chemical Name:(hydroxydimesitylsilyl)dimesitylgermane
CAS No.:154079-39-7
Molecular Formula:C₃₆H₄₆GeOSi
Molecular Weight:595.436
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (hydroxydimesitylsilyl)dimesitylgermane

Chemical Property:

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Technology Process of (hydroxydimesitylsilyl)dimesitylgermane

There total 2 articles about (hydroxydimesitylsilyl)dimesitylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 617-86-7
triethylsilane

: 136131-68-5
hexamesitylsiladigermirane

: 144435-57-4
dimesityl(triethylsilyl)germane

: 154079-39-7
(hydroxydimesitylsilyl)dimesitylgermane

Guidance literature:: With water; In acetone; toluene; Irradiation (UV/VIS); photolysis (350 nm) of a soln. of SiGe2Mes6 and Et3SiH in toluene for 8 h at -70°C, quenching with acetone containing traces of water; prarative TLC;
DOI:10.1021/om00014a038

Reference yield:

: 136131-68-5
hexamesitylsiladigermirane

: 154079-41-1
(hydroxydimesitylgermyl)dimesitylgermane

: 154079-40-0
(dimesitylsilyl)hydroxydimesitylgermane

: 154079-39-7
(hydroxydimesitylsilyl)dimesitylgermane

Guidance literature:: With water; In toluene; bubbling argon through a mixt. of SiGe2Mes6 and excess water, sealing the vessel, heating to 105°C for 16 h with intermittent shaking; removal of the solvent, preparative TLC;
DOI:10.1021/om00014a038