(hydroxydimesitylgermyl)dimesitylgermane

Base Information

Chemical Name:(hydroxydimesitylgermyl)dimesitylgermane
CAS No.:154079-41-1
Molecular Formula:C₃₆H₄₆Ge₂O
Molecular Weight:639.941
Hs Code.:

Synonyms:(hydroxydimesitylgermyl)dimesitylgermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (hydroxydimesitylgermyl)dimesitylgermane

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Technology Process of (hydroxydimesitylgermyl)dimesitylgermane

There total 7 articles about (hydroxydimesitylgermyl)dimesitylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 107824-84-0
hexamesitylcyclotrigermane

: 154079-41-1
(hydroxydimesitylgermyl)dimesitylgermane

Guidance literature:: With water; In toluene; degassing a mixt. of Ge3Mes6 and excess water in toluene, placing under argon, heating to 105°C for 16 h with periodic shaking during the first 6 h; removal of the solvent, preparative TLC;
DOI:10.1021/om00014a038

Reference yield: 55.0%

: 115385-07-4
tetrakis(2,4,6-trimethylphenyl)digermene

: 939-90-2
trans-2-phenylcyclopropane-1-carboxylic acid

: 154079-41-1
(hydroxydimesitylgermyl)dimesitylgermane

: ((CH₃)3C₆H₂)2Ge(OCOCHCH₂HC₆H₅C)GeH(C₆H₂(CH₃)3)2

Guidance literature:: In tetrahydrofuran; (N2); dissolving of trans-2-phenylcyclopropane-1-carboxylic acid in THF;addn. to soln. of (mesityl)4Ge2 in THF; stirring for 5 min at room temp .; chromy. (silica gel; 70/30 CH2Cl2/hexanes); as oil;
DOI:10.1021/om7005358

Reference yield: 55.0%

: 115385-07-4
tetrakis(2,4,6-trimethylphenyl)digermene

: 480-63-7
mesitylenecarboxylic acid

: 154079-41-1
(hydroxydimesitylgermyl)dimesitylgermane

: 957878-49-8
((CH₃)3C₆H₂)2Ge(OCOC₆H₂(CH₃)3)GeH(C₆H₂(CH₃)3)2

Guidance literature:: In tetrahydrofuran; (N2); dissolving of 2,4,6-trimethylbenzoic acid in THF; addn. to soln. of (mesityl)4Ge2 in THF for 1 min at room temp.; removal of solvent by rotary evapn.; chromy. (silica gel; 70/30 CH2Cl2/hexanes);
DOI:10.1021/om7005358