ethyl hept-3-ylideneamino)-2-phenylethyl>phosphinate

Base Information

Chemical Name:ethyl hept-3-ylideneamino)-2-phenylethyl>phosphinate
CAS No.:125472-60-8
Molecular Formula:C₂₅H₄₀NO₅P
Molecular Weight:465.57
Hs Code.:

ethyl <diethoxymethyl-(1S,2S,5S,1'S)-1-(2-hydroxy-2,6,6-trimethylbicyclo<3.1.1>hept-3-ylideneamino)-2-phenylethyl>phosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl hept-3-ylideneamino)-2-phenylethyl>phosphinate

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Technology Process of ethyl hept-3-ylideneamino)-2-phenylethyl>phosphinate

There total 4 articles about ethyl hept-3-ylideneamino)-2-phenylethyl>phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65600-74-0
ethyl diethoxymethylphosphinate

: 125472-60-8
ethyl hept-3-ylideneamino)-2-phenylethyl>phosphinate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 2 h / Heating

2: 74 percent / H₂ / 5percent Pd/C / ethanol / 20 h / 50 - 60 °C / 38000 - 45600 Torr

3: 7 percent / toluene / 120 °C

4: 1.) LDA / 1.) THF, -78 deg C, 2.) THF, 20 deg C

With hydrogen; lithium diisopropyl amide; palladium on activated charcoal; In ethanol; toluene;

Reference yield:

: 125402-10-0
ethyl benzhydrylaminomethyl(diethoxymethyl)phosphinate

: 125472-60-8
ethyl hept-3-ylideneamino)-2-phenylethyl>phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / H₂ / 5percent Pd/C / ethanol / 20 h / 50 - 60 °C / 38000 - 45600 Torr

2: 7 percent / toluene / 120 °C

3: 1.) LDA / 1.) THF, -78 deg C, 2.) THF, 20 deg C

With hydrogen; lithium diisopropyl amide; palladium on activated charcoal; In ethanol; toluene;

Reference yield:

: 125402-11-1
aminomethyl-(diethoxymethyl)-phosphinic acid ethyl ester

: 125472-60-8
ethyl hept-3-ylideneamino)-2-phenylethyl>phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 7 percent / toluene / 120 °C

2: 1.) LDA / 1.) THF, -78 deg C, 2.) THF, 20 deg C

With lithium diisopropyl amide; In toluene;