N-(6-nitroveratryloxycarbonyl)-4,7-difluorotryptophan cyanomethyl ester

Base Information

Chemical Name:N-(6-nitroveratryloxycarbonyl)-4,7-difluorotryptophan cyanomethyl ester
CAS No.:1393735-83-5
Molecular Formula:C₂₃H₂₀F₂N₄O₈
Molecular Weight:518.431
Hs Code.:

Synonyms:

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Chemical Property of N-(6-nitroveratryloxycarbonyl)-4,7-difluorotryptophan cyanomethyl ester

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Technology Process of N-(6-nitroveratryloxycarbonyl)-4,7-difluorotryptophan cyanomethyl ester

There total 5 articles about N-(6-nitroveratryloxycarbonyl)-4,7-difluorotryptophan cyanomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₁₉F₂N₃O₈

: 107-14-2
chloroacetonitrile

: 1393735-83-5
N-(6-nitroveratryloxycarbonyl)-4,7-difluorotryptophan cyanomethyl ester

Guidance literature:: With triethylamine; In dimethyl sulfoxide; at 20 ℃; for 5h;
DOI:10.1021/cb300246j

Reference yield:

: C₁₃H₁₄F₂N₂O₂

: 1393735-83-5
N-(6-nitroveratryloxycarbonyl)-4,7-difluorotryptophan cyanomethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / tetrahydrofuran; water / 3 h / 20 °C

2: sodium hydroxide / 1,4-dioxane / 0.25 h

3: triethylamine / dimethyl sulfoxide / 5 h / 20 °C

With sodium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide;
DOI:10.1021/cb300246j

Reference yield:

: 1393735-81-3
ethyl 3-(4,7-difluoro-1H-indol-3-yl)-2-(hydroxyimino)propanoate

: 1393735-83-5
N-(6-nitroveratryloxycarbonyl)-4,7-difluorotryptophan cyanomethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum/mercury amalgam; water / 1,4-dioxane / 24 h / 20 °C

2: sodium carbonate / tetrahydrofuran; water / 3 h / 20 °C

3: sodium hydroxide / 1,4-dioxane / 0.25 h

4: triethylamine / dimethyl sulfoxide / 5 h / 20 °C

With aluminum/mercury amalgam; water; sodium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide;
DOI:10.1021/cb300246j