2-methoxyethyl-N,N-bis(2-toluene-p-sulfonylaminoethyl)amine

Base Information

Chemical Name:2-methoxyethyl-N,N-bis(2-toluene-p-sulfonylaminoethyl)amine
CAS No.:144918-63-8
Molecular Formula:C₂₁H₃₁N₃O₅S₂
Molecular Weight:469.626
Hs Code.:

Synonyms:

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Chemical Property of 2-methoxyethyl-N,N-bis(2-toluene-p-sulfonylaminoethyl)amine

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Technology Process of 2-methoxyethyl-N,N-bis(2-toluene-p-sulfonylaminoethyl)amine

There total 1 articles about 2-methoxyethyl-N,N-bis(2-toluene-p-sulfonylaminoethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 3634-89-7
N-(p-toluenesulfonyl)aziridine

: 109-85-3
2-methoxyethylamine

: 144918-63-8
2-methoxyethyl-N,N-bis(2-toluene-p-sulfonylaminoethyl)amine

Guidance literature:: In acetonitrile; for 72h; Ambient temperature;
DOI:10.1039/DT9920002809

Reference yield: 79.0%

: 19439-55-5
AlEt₂(2-aminoethoxide)

: 144918-63-8
2-methoxyethyl-N,N-bis(2-toluene-p-sulfonylaminoethyl)amine

: 1215088-48-4
[Al(2-aminoethoxide)((N(Ts)CH₂CH₂)2NCH₂CH₂OMe)]

Guidance literature:: In toluene; (inert atm.); heating mixt. of aluminium compd. and sulfonamide deriv. itoluene at 100°C for 16 h; evapn., washing with pentane, drying in vac., elem. anal.;
DOI:10.1021/om901070g

Reference yield: 78.0%

: 16530-80-6
Ti(NMe₂)2(O-i-Pr)2

: 144918-63-8
2-methoxyethyl-N,N-bis(2-toluene-p-sulfonylaminoethyl)amine

: 1192571-98-4
Ti(MeOCH₂CH₂N(CH₂CH₂NSO₂Tol)2)(O-i-Pr₂)2

Guidance literature:: In dichloromethane; under inert atm. soln. ligand in CH2Cl2 was added to soln. Ti(NMe2)2(O-i-Pr)2 in CH2Cl2, stirred for 2 h; solvent was removed in vacuo, residue was recryst. from CH2Cl2 layered with pentane, ppt. was washed with pentane and dried in vacuo; elem. anal.;
DOI:10.1021/ic901524s