Technology Process of methyl varioside monobenzoate
There total 8 articles about methyl varioside monobenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
for 4h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 32 percent / pyridine
2: 81 percent / sodium, methanol / 2 h / Ambient temperature
3: 62 percent / pyridine / CH2Cl2 / 72 h / Ambient temperature
4: 75 percent / sodium, methanol / 3 h / Ambient temperature
5: 47 percent / lithium aluminium hydride / tetrahydrofuran / Heating
6: 65.5 percent / sodium hydride / tetrahydrofuran / 24.5 h / Ambient temperature
7: 79 percent / hydrogen, methanol / 5percent palladised carbon
8: 89 percent / pyridine / 4 h / Ambient temperature
With
pyridine; methanol; lithium aluminium tetrahydride; hydrogen; sodium; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 47 percent / lithium aluminium hydride / tetrahydrofuran / Heating
2: 65.5 percent / sodium hydride / tetrahydrofuran / 24.5 h / Ambient temperature
3: 79 percent / hydrogen, methanol / 5percent palladised carbon
4: 89 percent / pyridine / 4 h / Ambient temperature
With
pyridine; methanol; lithium aluminium tetrahydride; hydrogen; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran;
