Technology Process of C21H28N3O6P
There total 4 articles about C21H28N3O6P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium peroxoborate tetrahydrate;
In
methanol;
at 50 ℃;
for 1h;
DOI:10.1021/jm4006498
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 0.08 h / 175 °C / Microwave irradiation
2: sodium peroxoborate tetrahydrate / methanol / 1 h / 50 °C
With
tetrakis(triphenylphosphine) palladium(0); sodium peroxoborate tetrahydrate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm4006498
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 2 h / 20 °C
2: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 0.08 h / 175 °C / Microwave irradiation
3: sodium peroxoborate tetrahydrate / methanol / 1 h / 50 °C
With
tetrakis(triphenylphosphine) palladium(0); sodium peroxoborate tetrahydrate; triethylamine;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm4006498