N-{3-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tertbutyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-N',N'-di(tert-buthoxycarbonyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

Base Information

Chemical Name:N-{3-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tertbutyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-N',N'-di(tert-buthoxycarbonyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine
CAS No.:1154745-03-5
Molecular Formula:C₅₄H₇₇BrN₄O₈
Molecular Weight:990.131
Hs Code.:

N-{3-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tertbutyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-N',N'-di(tert-buthoxycarbonyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{3-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tertbutyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-N',N'-di(tert-buthoxycarbonyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

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Technology Process of N-{3-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tertbutyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-N',N'-di(tert-buthoxycarbonyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

There total 1 articles about N-{3-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tertbutyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-N',N'-di(tert-buthoxycarbonyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 854669-43-5
tert-butyl {3-{3-[3-(3-bromo-5-tert-butyl-2-methoxyphenyl)amino-5-tert-butyl-2-methoxyphenyl]amino-5-tert-butyl-2-methoxyphenyl}amino-5-tert-butyl-2-methoxyphenyl}carbamate

: 24424-99-5
di-tert-butyl dicarbonate

: 1154745-03-5
N-{3-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tertbutyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-N',N'-di(tert-buthoxycarbonyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

Guidance literature:: With dmap; In tetrahydrofuran; for 13h; Reflux;
DOI:10.1016/j.tetasy.2009.01.017

Reference yield:

: 1154745-03-5
N-{3-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tertbutyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-N',N'-di(tert-buthoxycarbonyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine

: 100-39-0
benzyl bromide

: C₇₅H₉₅BrN₄O₈

Guidance literature:: N-{3-[3-(3-bromo-5-tert-butyl-2-methoxyanilino)-5-tertbutyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-N',N'-di(tert-buthoxycarbonyl)-5-tert-butyl-2-methoxy-1,3-phenylenediamine; With sodium hydride; In N,N-dimethyl-formamide; at -20 ℃; for 0.25h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; at 0 ℃; for 8h; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.01.017