p-nitrophenyl t-butyloxycarbonylglycyl-m-aminomethylbenzoate

Base Information

Chemical Name:p-nitrophenyl t-butyloxycarbonylglycyl-m-aminomethylbenzoate
CAS No.:89760-89-4
Molecular Formula:C₂₁H₂₃N₃O₇
Molecular Weight:429.43
Hs Code.:

Synonyms:

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Chemical Property of p-nitrophenyl t-butyloxycarbonylglycyl-m-aminomethylbenzoate

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Technology Process of p-nitrophenyl t-butyloxycarbonylglycyl-m-aminomethylbenzoate

There total 5 articles about p-nitrophenyl t-butyloxycarbonylglycyl-m-aminomethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 89760-89-4
p-nitrophenyl t-butyloxycarbonylglycyl-m-aminomethylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / DCC

2: 90 percent / 2 M HBr / acetic acid / 1 h / Ambient temperature

3: 1.) isobutyl chloroformate, N-methylmorpholine, 2.) N-methylmorpholine / 1.) acetonotrile, 2.) acetonitrile

With 4-methyl-morpholine; hydrogen bromide; dicyclohexyl-carbodiimide; isobutyl chloroformate; In acetic acid;

Reference yield:

: 2393-20-6
3-aminomethylbenzoic acid

: 89760-89-4
p-nitrophenyl t-butyloxycarbonylglycyl-m-aminomethylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / triethylamine / dioxane; H₂O / 5 h

2: 100 percent / DCC

3: 90 percent / 2 M HBr / acetic acid / 1 h / Ambient temperature

4: 1.) isobutyl chloroformate, N-methylmorpholine, 2.) N-methylmorpholine / 1.) acetonotrile, 2.) acetonitrile

With 4-methyl-morpholine; hydrogen bromide; triethylamine; dicyclohexyl-carbodiimide; isobutyl chloroformate; In 1,4-dioxane; water; acetic acid;

Reference yield:

: 89760-77-0
3-<(benzyloxycarbonyl)aminomethyl>benzoic acid

: 89760-89-4
p-nitrophenyl t-butyloxycarbonylglycyl-m-aminomethylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / DCC

2: 90 percent / 2 M HBr / acetic acid / 1 h / Ambient temperature

3: 1.) isobutyl chloroformate, N-methylmorpholine, 2.) N-methylmorpholine / 1.) acetonotrile, 2.) acetonitrile

With 4-methyl-morpholine; hydrogen bromide; dicyclohexyl-carbodiimide; isobutyl chloroformate; In acetic acid;