(R_P)-N⁶-Benzoyl-5'-O--O^P-(4-chlorphenyl)-2'-desoxyadenylyl-(3'-5')-3'-O-acetyl-N⁶-benzoyl-2'-desoxyadenosin

Base Information

• Chemical Name: (R_P)-N⁶-Benzoyl-5'-O--O^P-(4-chlorphenyl)-2'-desoxyadenylyl-(3'-5')-3'-O-acetyl-N⁶-benzoyl-2'-desoxyadenosin
• CAS No.: 82893-27-4
• Molecular Formula: C₆₃H₅₆ClN₁₀O₁₃P
• Molecular Weight: 1227.62

Synonyms:

Chemical Property of (R_P)-N⁶-Benzoyl-5'-O--O^P-(4-chlorphenyl)-2'-desoxyadenylyl-(3'-5')-3'-O-acetyl-N⁶-benzoyl-2'-desoxyadenosin

Chemical Property:

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Technology Process of (R_P)-N⁶-Benzoyl-5'-O--O^P-(4-chlorphenyl)-2'-desoxyadenylyl-(3'-5')-3'-O-acetyl-N⁶-benzoyl-2'-desoxyadenosin

There total 10 articles about (R_P)-N⁶-Benzoyl-5'-O--O^P-(4-chlorphenyl)-2'-desoxyadenylyl-(3'-5')-3'-O-acetyl-N⁶-benzoyl-2'-desoxyadenosin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N6-benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine (64325-78-6) → (SP)-N6-Benzoyl-5'-O--OP-(4-chlorphenyl)-2'-desoxyadenylyl-(3'-5')-3'-O-acetyl-N6-benzoyl-2'-desoxyadenosin (82893-27-4,82916-93-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 2) 5 percent p-TsOH / 1) pyridine, room temp., 15 h, 2) CH₂Cl₂/methanol, 0 deg C, 15 min

2: mesitylenesulfonyltriazole / pyridine / 48 h / Ambient temperature

With mesitylenesulfonyltriazole; toluene-4-sulfonic acid; In pyridine;

Reference yield:

N6-benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine (64325-78-6) → (RP)-N6-Benzoyl-5'-O--OP-(4-chlorphenyl)-2'-desoxyadenylyl-(3'-5')-3'-O-acetyl-N6-benzoyl-2'-desoxyadenosin (82893-27-4,82916-93-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 2) 5 percent p-TsOH / 1) pyridine, room temp., 15 h, 2) CH₂Cl₂/methanol, 0 deg C, 15 min

2: mesitylenesulfonyltriazole / pyridine / 48 h / Ambient temperature

With mesitylenesulfonyltriazole; toluene-4-sulfonic acid; In pyridine;

Reference yield:

N6-benzoyl-2'-deoxyadenosine (4546-72-9) → (SP)-N6-Benzoyl-5'-O--OP-(4-chlorphenyl)-2'-desoxyadenylyl-(3'-5')-3'-O-acetyl-N6-benzoyl-2'-desoxyadenosin (82893-27-4,82916-93-6)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / 5 h / Ambient temperature

2: 2) 5 percent p-TsOH / 1) pyridine, room temp., 15 h, 2) CH₂Cl₂/methanol, 0 deg C, 15 min

3: mesitylenesulfonyltriazole / pyridine / 48 h / Ambient temperature

With mesitylenesulfonyltriazole; toluene-4-sulfonic acid; In pyridine;

upstream raw materials:

4,4'-dimethoxytrityl chloride

p-chlorophenyl phosphoroditriazolide

N₆-benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine

N₆-benzoyl-2'-deoxyadenosine

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