(2S)-1,2-Pyrrolidinedicarboxylic acid 2-(pentachlorophenyl)1-benzyl ester

Base Information

• Chemical Name: (2S)-1,2-Pyrrolidinedicarboxylic acid 2-(pentachlorophenyl)1-benzyl ester
• CAS No.: 13673-56-8
• Molecular Formula: C19H14Cl5NO4
• Molecular Weight: 497.58400
• Mol file: 13673-56-8.mol

Synonyms:Z-Pro-ONp;(S)-Pyrrolidine-1,2-dicarboxylic acid 1-benzyl ester 2-pentachlorophenyl ester;

Chemical Property of (2S)-1,2-Pyrrolidinedicarboxylic acid 2-(pentachlorophenyl)1-benzyl ester

Chemical Property:

• PSA: 55.84000
• LogP: 6.59810

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2S)-1,2-Pyrrolidinedicarboxylic acid 2-(pentachlorophenyl)1-benzyl ester

There total 1 articles about (2S)-1,2-Pyrrolidinedicarboxylic acid 2-(pentachlorophenyl)1-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Carbobenzoxyprolin-pentachlorphenylester (13673-56-8,36727-76-1)

Guidance literature:

Carbobenzoxyprolin, Pentachlorphenol, Carbodiimid;

Reference yield:

HBr*H-L-Ser-L-Tyr-D-Ala-L-Leu-OMe + Z-Pro-OPcp (13673-56-8) → Z-L-Pro-L-Ser-L-Tyr-D-Ala-L-Leu-OMe (77659-15-5)

Guidance literature:

With 4-methyl-morpholine; In N,N-dimethyl-formamide; for 48h; Ambient temperature;

DOI:10.1007/BF00579436

Reference yield:

Z-Pro-OPcp (13673-56-8) + [({[2-(2-{[(S)-1-((S)-2-Amino-3-phenyl-propionyl)-pyrrolidine-2-carbonyl]-amino}-acetylamino)-ethylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamic acid tert-butyl ester (161403-99-2) → Z-Pro-Phe-Pro-Gly-EtDA<*>Gly<*>Gly-Boc (161404-00-8)

Guidance literature:

In N,N-dimethyl-formamide; Yield given;

Downstream raw materials:

benzyloxycarbonyl-L-prolin-L-valin methyl ester

Z-L-Pro-L-Ser-L-Tyr-D-Ala-L-Leu-OMe

Z-Pro-Phe-Pro-Gly-EtDA<*>Gly<*>Gly-Boc

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