7-chloro-3-<2,3-dideoxy-5-O-<(dimethylethyl)diphenylsilyl>-β-D-glycero-pentofuranosyl>-3H-1,2,3-triazolo<4,5-b>pyridine

Base Information

• Chemical Name: 7-chloro-3-<2,3-dideoxy-5-O-<(dimethylethyl)diphenylsilyl>-β-D-glycero-pentofuranosyl>-3H-1,2,3-triazolo<4,5-b>pyridine
• CAS No.: 162299-73-2
• Molecular Formula: C₂₆H₂₉ClN₄O₂Si
• Molecular Weight: 493.08
• Mol file: 162299-73-2.mol

Synonyms:

Chemical Property of 7-chloro-3-<2,3-dideoxy-5-O-<(dimethylethyl)diphenylsilyl>-β-D-glycero-pentofuranosyl>-3H-1,2,3-triazolo<4,5-b>pyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-chloro-3-<2,3-dideoxy-5-O-<(dimethylethyl)diphenylsilyl>-β-D-glycero-pentofuranosyl>-3H-1,2,3-triazolo<4,5-b>pyridine

There total 1 articles about 7-chloro-3-<2,3-dideoxy-5-O-<(dimethylethyl)diphenylsilyl>-β-D-glycero-pentofuranosyl>-3H-1,2,3-triazolo<4,5-b>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

7-chloro-3H-1,2,3-triazolo<4,5-b>pyridine (34550-49-7) + 2,3-dideoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-α-D-glycero-pentofuranosyl chloride (134965-83-6,135092-93-2) → 7-chloro-2-<2,3-dideoxy-5-O-<(dimethylethyl)diphenylsilyl>-β-D-glycero-pentofuranosyl>-2H-1,2,3-triazolo<4,5-b>pyridine + 7-chloro-1-<2,3-dideoxy-5-O-<(dimethylethyl)diphenylsilyl>-α-D-glycero-pentofuranosyl>-1H-1,2,3-triazolo<4,5-b>pyridine + 7-chloro-3-<2,3-dideoxy-5-O-<(dimethylethyl)diphenylsilyl>-α-D-glycero-pentofuranosyl>-3H-1,2,3-triazolo<4,5-b>pyridine (162181-04-6) + 7-chloro-3-<2,3-dideoxy-5-O-<(dimethylethyl)diphenylsilyl>-β-D-glycero-pentofuranosyl>-3H-1,2,3-triazolo<4,5-b>pyridine (162299-73-2)

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; acetonitrile; for 5h; Yields of byproduct given; Ambient temperature;

DOI:10.1080/15257779408009477

upstream raw materials:

7-chloro-3H-1,2,3-triazolo<4,5-b>pyridine

2,3-dideoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-α-D-glycero-pentofuranosyl chloride