(cycloocta-1,5-diene)(maleic anhydride)nickel

Base Information

• Chemical Name: (cycloocta-1,5-diene)(maleic anhydride)nickel
• CAS No.: 91158-57-5
• Molecular Formula: C₁₂H₁₄NiO₃
• Molecular Weight: 264.931
• Mol file: 91158-57-5.mol

Synonyms:

Chemical Property of (cycloocta-1,5-diene)(maleic anhydride)nickel

Chemical Property:

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Technology Process of (cycloocta-1,5-diene)(maleic anhydride)nickel

There total 1 articles about (cycloocta-1,5-diene)(maleic anhydride)nickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

maleic anhydride (108-31-6) + (cycloocta-1,5-diene)(methyl trans-β-(phenylsulfonyl)acrylate)nickel (91158-50-8) → (cycloocta-1,5-diene)(maleic anhydride)nickel (91158-57-5) + (E)-β-methoxycarbonylvinyl phenyl sulphone (1865-13-0)

Guidance literature:

In tetrahydrofuran; To a stirred soln. of complex in THF was added dropwise a soln. of ligand in THF at -20°C., the soln. was stirred for ca. 1 h (Ar atm.);; recrystd. from Et2O-THF at -20°C; elem. anal.;;

upstream raw materials:

maleic anhydride

(cycloocta-1,5-diene)(methyl trans-β-(phenylsulfonyl)acrylate)nickel