[1-Phenanthren-2-yl-meth-(E)-ylidene]-(4-tetradecyloxy-phenyl)-amine

Base Information

• Chemical Name: [1-Phenanthren-2-yl-meth-(E)-ylidene]-(4-tetradecyloxy-phenyl)-amine
• CAS No.: 104952-88-7
• Molecular Formula: C₃₅H₄₃NO
• Molecular Weight: 493.733
• Mol file: 104952-88-7.mol

Synonyms:

Chemical Property of [1-Phenanthren-2-yl-meth-(E)-ylidene]-(4-tetradecyloxy-phenyl)-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [1-Phenanthren-2-yl-meth-(E)-ylidene]-(4-tetradecyloxy-phenyl)-amine

There total 6 articles about [1-Phenanthren-2-yl-meth-(E)-ylidene]-(4-tetradecyloxy-phenyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenanthrene (85-01-8) → [1-Phenanthren-2-yl-meth-(E)-ylidene]-(4-tetradecyloxy-phenyl)-amine (104952-88-7)

Guidance literature:

Multi-step reaction with 6 steps

1: 14 percent / aluminium chloride / nitrobenzene / 8.5 h / 0 - 25 °C

2: 55 percent / 2percent sodium hypochlorite / H₂O / 24 h / Heating

3: 87 percent / 12percent boron trifluoride / 6 h / Heating

4: 93 percent / lithium aluminium hydride / diethyl ether / 0.5 h / Heating

5: 85 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h / Ambient temperature

With sodium hypochlorite; lithium aluminium tetrahydride; aluminium trichloride; boron trifluoride; pyridinium chlorochromate; In diethyl ether; dichloromethane; water; nitrobenzene;

Reference yield:

2-acetylphenanthrene (5960-69-0) → [1-Phenanthren-2-yl-meth-(E)-ylidene]-(4-tetradecyloxy-phenyl)-amine (104952-88-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 55 percent / 2percent sodium hypochlorite / H₂O / 24 h / Heating

2: 87 percent / 12percent boron trifluoride / 6 h / Heating

3: 93 percent / lithium aluminium hydride / diethyl ether / 0.5 h / Heating

4: 85 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h / Ambient temperature

With sodium hypochlorite; lithium aluminium tetrahydride; boron trifluoride; pyridinium chlorochromate; In diethyl ether; dichloromethane; water;

Reference yield:

phenanthrene-2-carboxylic acid (40452-20-8) → [1-Phenanthren-2-yl-meth-(E)-ylidene]-(4-tetradecyloxy-phenyl)-amine (104952-88-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 87 percent / 12percent boron trifluoride / 6 h / Heating

2: 93 percent / lithium aluminium hydride / diethyl ether / 0.5 h / Heating

3: 85 percent / pyridinium chlorochromate / CH₂Cl₂ / 2 h / Ambient temperature

With lithium aluminium tetrahydride; boron trifluoride; pyridinium chlorochromate; In diethyl ether; dichloromethane;

upstream raw materials:

phenanthrene-2-carbaldehyde

4-(tetradecyloxy)aniline

phenanthrene

2-acetylphenanthrene