C₂₈H₃₉NO₂Si

Base Information

• Chemical Name: C₂₈H₃₉NO₂Si
• CAS No.: 935673-59-9
• Molecular Formula: C₂₈H₃₉NO₂Si
• Molecular Weight: 449.709
• Mol file: 935673-59-9.mol

Synonyms:

Chemical Property of C₂₈H₃₉NO₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₃₉NO₂Si

There total 3 articles about C₂₈H₃₉NO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H29BrMgOSi → C28H39NO2Si (935673-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: MeMgCl / tetrahydrofuran / 0 - 20 °C

1.2: tetrahydrofuran / 12 h / 20 °C

1.3: 65 percent / NaBH₃CN; HOAc / tetrahydrofuran / 0.75 h / 20 °C

2.1: CH₂Cl₂ / 10 h / 20 °C

With methylmagnesium chloride; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jo062533h

Reference yield:

piperidine-2,6-dione (1121-89-7) → C28H39NO2Si (935673-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: MeMgCl / tetrahydrofuran / 0 - 20 °C

1.2: tetrahydrofuran / 12 h / 20 °C

1.3: 65 percent / NaBH₃CN; HOAc / tetrahydrofuran / 0.75 h / 20 °C

2.1: CH₂Cl₂ / 10 h / 20 °C

With methylmagnesium chloride; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jo062533h

Reference yield:

C27H37NO2Si (935673-58-8) + methyl trifluoromethanesulfonate (333-27-7) → C28H39NO2Si (935673-59-9)

Guidance literature:

In dichloromethane; at 20 ℃; for 10h;

DOI:10.1021/jo062533h

upstream raw materials:

C₂₇H₃₇NO₂Si

methyl trifluoromethanesulfonate

piperidine-2,6-dione

Downstream raw materials:

C₃₃H₄₃NO₅Si