PdI₂((C₆H₁₁)2PCH₂P(C₆H₁₁)2)

Base Information

Chemical Name:PdI₂((C₆H₁₁)2PCH₂P(C₆H₁₁)2)
CAS No.:295325-15-4
Molecular Formula:C₂₅H₄₆I₂P₂Pd
Molecular Weight:768.817
Hs Code.:

PdI<sub>2</sub>((C<sub>6</sub>H<sub>11</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>11</sub>)2)

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of PdI₂((C₆H₁₁)2PCH₂P(C₆H₁₁)2)

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Technology Process of PdI₂((C₆H₁₁)2PCH₂P(C₆H₁₁)2)

There total 2 articles about PdI₂((C₆H₁₁)2PCH₂P(C₆H₁₁)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 295325-16-5
Pd(dcpm)Cl₂

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 295325-15-4
PdI₂((C₆H₁₁)2PCH₂P(C₆H₁₁)2)

Guidance literature:: In toluene; (N2); addn. of NaI to a slurry of palladium complex in toluene, stirring at 20 °C for 30 min; decantation, washing with ether, drying under vac., recrystn. (CH2Cl2-ether) at -25 °C; elem. anal.;
DOI:10.1021/om000350u

Reference yield:

: C₆H₅PdI((C₆H₁₁)2PCH₂P(C₆H₁₁)2)*CH₂Cl₂

: 829-85-6
diphenylphosphane

: 295325-15-4
PdI₂((C₆H₁₁)2PCH₂P(C₆H₁₁)2)

: 295325-06-3
[(C₆H₅)2PHPdP(C₆H₅)2PdP(C₆H₅)2H((C₆H₁₁)2PCH₂P(C₆H₁₁)2)]⁽¹⁺⁾*I^(1-)=[((C₆H₅)2PH)2PdP(C₆H₅)2Pd((C₆H₁₁)2PCH₂P(C₆H₁₁)2)]I

Guidance literature:: In tetrahydrofuran; (N2); addn. of phosphine to a slurry of palladium complex in THF, keeping for 12 h at 20 °C; filtration, evapn., redissolving in toluene, filtration, keeping at room temp. for 2 d;
DOI:10.1021/om000350u