C₂₉H₃₂O₇S

Base Information

• Chemical Name: C₂₉H₃₂O₇S
• CAS No.: 75885-04-0
• Molecular Formula: C₂₉H₃₂O₇S
• Molecular Weight: 524.635
• Mol file: 75885-04-0.mol

Synonyms:

Chemical Property of C₂₉H₃₂O₇S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₂O₇S

There total 1 articles about C₂₉H₃₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl(chlorophenylmethylene)ammonium chloride (2397-26-4) + 3-epi-gibberellin A1 methyl ester 13-acetate (75884-90-1) → N,N-dimethylthiobenzamide (15482-60-7) + C29H32O7S (75885-04-0)

Guidance literature:

With hydrogen sulfide; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, THF, 18 deg C, 50 h, 2.) pyridine, 5 min;

Reference yield:

C29H32O7S (75885-04-0) → gibberellin A20 methyl ester (15355-41-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 16 mg / tri-n-butylstannane, 2,2'-azobis(2-methylpropionitrile) / toluene / Heating

2: 2M NaOH / methanol / 1.) reflux, 16 h, 2.) 18 deg C, 3 d

With sodium hydroxide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In methanol; toluene;

Reference yield:

C29H32O7S (75885-04-0) → GA20 (19143-87-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 16 mg / tri-n-butylstannane, 2,2'-azobis(2-methylpropionitrile) / toluene / Heating

2: 47 mg / 2M NaOH / methanol / 1.) reflux, 16 h, 2.) 18 deg C, 3 d

With sodium hydroxide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In methanol; toluene;

upstream raw materials:

N,N-dimethyl(chlorophenylmethylene)ammonium chloride

3-epi-gibberellin A₁ methyl ester 13-acetate

Downstream raw materials:

GA₂₀

gibberellin A₂₀ methyl ester

gibberellin A₅

Refernces