2-[({2-[3,25-dioxa-11.14.17.31-tetrazatetracyclo[25.3.1.0^4,9.0^19,24]hentriaconta-1⁽³⁰⁾.4⁽⁹⁾.5.7.19⁽²⁴⁾.20.22.27⁽³¹⁾.28-nonaen-14-yl]ethyl}imino)methyl]phenol

Base Information

• Chemical Name: 2-[({2-[3,25-dioxa-11.14.17.31-tetrazatetracyclo[25.3.1.0^4,9.0^19,24]hentriaconta-1⁽³⁰⁾.4⁽⁹⁾.5.7.19⁽²⁴⁾.20.22.27⁽³¹⁾.28-nonaen-14-yl]ethyl}imino)methyl]phenol
• CAS No.: 696587-23-2
• Molecular Formula: C₃₄H₃₉N₅O₃
• Molecular Weight: 565.715

Synonyms:

Chemical Property of 2-[({2-[3,25-dioxa-11.14.17.31-tetrazatetracyclo[25.3.1.0^4,9.0^19,24]hentriaconta-1⁽³⁰⁾.4⁽⁹⁾.5.7.19⁽²⁴⁾.20.22.27⁽³¹⁾.28-nonaen-14-yl]ethyl}imino)methyl]phenol

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Technology Process of 2-[({2-[3,25-dioxa-11.14.17.31-tetrazatetracyclo[25.3.1.0^4,9.0^19,24]hentriaconta-1⁽³⁰⁾.4⁽⁹⁾.5.7.19⁽²⁴⁾.20.22.27⁽³¹⁾.28-nonaen-14-yl]ethyl}imino)methyl]phenol

There total 4 articles about 2-[({2-[3,25-dioxa-11.14.17.31-tetrazatetracyclo[25.3.1.0^4,9.0^19,24]hentriaconta-1⁽³⁰⁾.4⁽⁹⁾.5.7.19⁽²⁴⁾.20.22.27⁽³¹⁾.28-nonaen-14-yl]ethyl}imino)methyl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[3,25-dioxa-11.14.17.31-tetrazatetracyclo[25.3.1.04,9.019,24]hentriaconta-1(31).4(9).5.7.10.17.19(24).20.22.27.29-nonaen-14-yl]-1-ethanamine → 2-[({2-[3,25-dioxa-11.14.17.31-tetrazatetracyclo[25.3.1.04,9.019,24]hentriaconta-1(30).4(9).5.7.19(24).20.22.27(31).28-nonaen-14-yl]ethyl}imino)methyl]phenol (696587-23-2)

Guidance literature:

Multi-step reaction with 2 steps

1: NaBH₄ / methanol

2: ethanol / 4 h / Heating

With sodium tetrahydroborate; In methanol; ethanol;

DOI:10.1139/v03-214

Reference yield:

2,6-Bis(2-formylphenoxymethyl)pyridine (66433-95-2) → 2-[({2-[3,25-dioxa-11.14.17.31-tetrazatetracyclo[25.3.1.04,9.019,24]hentriaconta-1(30).4(9).5.7.19(24).20.22.27(31).28-nonaen-14-yl]ethyl}imino)methyl]phenol (696587-23-2)

Guidance literature:

Multi-step reaction with 3 steps

1: Ba(ClO₄)*xH₂O / methanol / 6 h / Heating

2: NaBH₄ / methanol

3: ethanol / 4 h / Heating

With sodium tetrahydroborate; Ba⁽²⁺⁾*ClO₄^(1-)=BaClO₄⁽¹⁺⁾; In methanol; ethanol;

DOI:10.1139/v03-214

Reference yield:

2,2',2''-triaminotriethylamine (4097-89-6) → 2-[({2-[3,25-dioxa-11.14.17.31-tetrazatetracyclo[25.3.1.04,9.019,24]hentriaconta-1(30).4(9).5.7.19(24).20.22.27(31).28-nonaen-14-yl]ethyl}imino)methyl]phenol (696587-23-2)

Guidance literature:

Multi-step reaction with 3 steps

1: Ba(ClO₄)*xH₂O / methanol / 6 h / Heating

2: NaBH₄ / methanol

3: ethanol / 4 h / Heating

With sodium tetrahydroborate; Ba⁽²⁺⁾*ClO₄^(1-)=BaClO₄⁽¹⁺⁾; In methanol; ethanol;

DOI:10.1139/v03-214

upstream raw materials:

2-[3.25-dioxa-11.14.17.31-tetraazatetracyclo[25.3.1.O(4.9).O(19.24)]hentriaconta-1⁽³¹⁾.4⁽⁹⁾.5.7.10.17.19⁽²⁴⁾.20.22.27.29-nonaen-14-yl]-1-athanamine

2-methyl-benzyl alcohol

2,6-Bis(2-formylphenoxymethyl)pyridine

2,2',2''-triaminotriethylamine

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