2-<3-propyl> acetate

Base Information

• Chemical Name: 2-<3-propyl> acetate
• CAS No.: 147912-86-5
• Molecular Formula: C₁₂H₁₄F₂O₃Se
• Molecular Weight: 323.198

Synonyms:

Chemical Property of 2-<3-propyl> acetate

Chemical Property:

Purity/Quality:

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Technology Process of 2-<3-propyl> acetate

There total 4 articles about 2-<3-propyl> acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Difluoromethyl phenyl selenide (101220-61-5) → 2-<3-propyl> acetate (147912-86-5)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂O₂ / CH₂Cl₂

2: CH₂Cl₂ / Heating

3: CH₂Cl₂ / Heating

With dihydrogen peroxide; In dichloromethane;

DOI:10.1016/S0040-4039(00)91782-9

Reference yield:

sodium phenylselenide (23974-72-3) → 2-<3-propyl> acetate (147912-86-5)

Guidance literature:

Multi-step reaction with 4 steps

1: ethanol; dimethylformamide

2: H₂O₂ / CH₂Cl₂

3: CH₂Cl₂ / Heating

4: CH₂Cl₂ / Heating

With dihydrogen peroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)91782-9

Reference yield:

acetic anhydride (108-24-7) + Difluoromethyl phenyl selenoxide (147912-92-3) + methyloxirane (75-56-9,16033-71-9) → 2-<3-propyl> acetate (147912-86-5) + 2-propyl acetate (147912-85-4)

Guidance literature:

In dichloromethane; for 4h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;

DOI:10.1021/jo00107a016

upstream raw materials:

C₁₁H₁₂F₂O₄Se

methyloxirane

acetic anhydride

Difluoromethyl phenyl selenoxide

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