2-methoxyethyl 4-trifluoromethylbenzenesulfenate

Base Information

Chemical Name:2-methoxyethyl 4-trifluoromethylbenzenesulfenate
CAS No.:197074-11-6
Molecular Formula:C₁₀H₁₁F₃O₂S
Molecular Weight:252.257
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methoxyethyl 4-trifluoromethylbenzenesulfenate

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Technology Process of 2-methoxyethyl 4-trifluoromethylbenzenesulfenate

There total 1 articles about 2-methoxyethyl 4-trifluoromethylbenzenesulfenate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 825-83-2
4-trifluoromethylbenzenethiol

: 197074-11-6
2-methoxyethyl 4-trifluoromethylbenzenesulfenate

Guidance literature:: Multi-step reaction with 2 steps

1: Cl₂ / CCl₄ / 1 h / 0 °C

2: Et₃N / diethyl ether / 0.5 h / 0 °C

With chlorine; triethylamine; In tetrachloromethane; diethyl ether;
DOI:10.1080/00032719808006489

Reference yield:

: 160455-46-9
(E)-2-(3,4-Dimethoxy-benzyl)-4,8-dimethyl-nona-3,7-dienenitrile

: 197074-11-6
2-methoxyethyl 4-trifluoromethylbenzenesulfenate

: (4bR,7R,8aS,9S)-2,3-Dimethoxy-4b,8,8-trimethyl-7-(4-trifluoromethyl-phenylsulfanyl)-4b,5,6,7,8,8a,9,10-octahydro-phenanthrene-9-carbonitrile

: (4bR,7R,8aS,9R)-2,3-Dimethoxy-4b,8,8-trimethyl-7-(4-trifluoromethyl-phenylsulfanyl)-4b,5,6,7,8,8a,9,10-octahydro-phenanthrene-9-carbonitrile

Guidance literature:: With boron trifluoride nitrometane adduct; In nitromethane; at -20 ℃; for 0.0833333h; Yield given. Yields of byproduct given;
DOI:10.1021/jo970451a