(η(5):η(1)-C5H4CH2CH2PPh2)IrI2

Base Information

Chemical Name:(η(5):η(1)-C5H4CH2CH2PPh2)IrI2
CAS No.:157047-10-4
Molecular Formula:C₁₉H₁₈I₂IrP
Molecular Weight:723.355
Hs Code.:

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Chemical Property of (η(5):η(1)-C5H4CH2CH2PPh2)IrI2

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Technology Process of (η(5):η(1)-C5H4CH2CH2PPh2)IrI2

There total 1 articles about (η(5):η(1)-C5H4CH2CH2PPh2)IrI2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 157047-04-6
(η(5):η(1)-C5H4CH2CH2PPh2)Ir(η(2)-C2H4)

: 157047-10-4
(η(5):η(1)-C5H4CH2CH2PPh2)IrI2

Guidance literature:: With I₂; In dichloromethane; under N2 or Ar; I2/CH2Cl2 added to the soln. of the Ir-complex in CH2Cl2 at room temp., soln. stirred (1 h), giving a red-brown soln.; evapn., recrystn. (CH2Cl2/Et2O), elem. anal.;

Reference yield: 75.0%

: 157047-10-4
(η(5):η(1)-C5H4CH2CH2PPh2)IrI2

: 2966-50-9
silver trifluoroacetate

: 191488-96-7
(η(5):η(1)-C5H4CH2CH2PPh2)Ir(CF3COO)2

Guidance literature:: In dichloromethane; inert atmosphere; addn. of Ir-complex to 2 equiv. of Ag-salt, stirring for 30 min; filtration, solvent removal (vac.), crystn. (pentane/PhMe); elem. anal.;
DOI:10.1016/S0022-328X(96)06803-9