Na[Mo2Cp2(μ-PPh2)(μ-CO)2]

Base Information

Chemical Name:Na[Mo2Cp2(μ-PPh2)(μ-CO)2]
CAS No.:537683-67-3
Molecular Formula:C₂₄H₂₀Mo₂O₂P*Na
Molecular Weight:586.265
Hs Code.:

Synonyms:

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Chemical Property of Na[Mo2Cp2(μ-PPh2)(μ-CO)2]

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Technology Process of Na[Mo2Cp2(μ-PPh2)(μ-CO)2]

There total 1 articles about Na[Mo2Cp2(μ-PPh2)(μ-CO)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 537683-60-6
[Mo2Cp2(μ-Cl)(μ-PPh2)(CO)2]

: 537683-67-3
Na[Mo2Cp2(μ-PPh2)(μ-CO)2]

Guidance literature:: With sodium amalgam; In tetrahydrofuran; (N2, Schlenk) the soln. of complex in THF was stirred with an excess of sodium amalgam for ca. 15 min; not isolated;
DOI:10.1039/b909493h

Reference yield: 62.0%

: [Re(η⁵-C₅H₄Me)(CO)₂(NO)]BF₄

: 537683-67-3
Na[Mo2Cp2(μ-PPh2)(μ-CO)2]

: [Mo2ReCp2(η5-C5H4Me)(μ-N)(μ-O)(μ-PPh2)(CO)4]

Guidance literature:: In tetrahydrofuran; (N2) Re complex was added at 193 K to soln. Mo complex in THF, stirred for 30 min and allowed to warm to 243 K; solvent was removed in vacuo, residue was extd. with CH2Cl2 and chromd. on alumina (CH2Cl2 - petroleum ether 1:1) at 243 K, solvent was removed at 243 K;
DOI:10.1021/ic901120x

Reference yield: 27.0%

: 537683-67-3
Na[Mo2Cp2(μ-PPh2)(μ-CO)2]

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 80-11-5
N-methyl-N-nitrosotoluene-p-sulfonamide

: [Mo2Cp2(μ-PPh2)(μ-η1:η2-CN-t-Bu)(CO)(NO)]

: 1190770-42-3
[Mo2Cp2(μ-PPh2)(CN-t-Bu)(CO)2(NO)]

Guidance literature:: In tetrahydrofuran; (N2) N-methyl-N-nitroso-p-toluenesulfonamide and CN-t-Bu were added at 203 K to soln. Mo complex in THF, stirred for 90 min, allowed to warm to roomtemp.; solvent was removed in vacuo, residue was extd. with toluene and chromd.on alumina at 285 K; elem. anal.;
DOI:10.1021/ic901120x